Purification of active bufadienolides from toad skin by preparative reversed-phase liquid chromatography coupled with hydrophilic interaction chromatography

Journal of Separation Science

Volumn 33, Issue 10, 2010, Pages 1487-1494

  Liu, Yanfang ^a   Feng, Jiatao ^a   Xiao, Yuansheng ^a   Guo, Zhimou ^a   Zhang, Jing ^a   Xue, Xingya ^a   Ding, Jin ^b   Zhang, Xiuli ^a   Liang, Xinmiao ^a  

^a DALIAN INSTITUTE OF CHEMICAL PHYSICS   (China)

^b SECOND MILITARY MEDICAL UNIVERSITY   (China)

Author keywords

Bufadienolides; Cyclodextrin; Hydrophilic interaction chromatography; Purification; Reversed phase liquid chromatography

Indexed keywords

ACTIVE COMPOUNDS; CRUDE SAMPLES; HIGH PURITY; HYDROPHILIC INTERACTION CHROMATOGRAPHY; INTEGRATED METHOD; NATURAL PRODUCTS; REVERSED-PHASE LIQUID CHROMATOGRAPHY;

HYDROPHILICITY; LIQUIDS; PURIFICATION; STEREOCHEMISTRY;

LIQUID CHROMATOGRAPHY;

BETA CYCLODEXTRIN; BUFADIENOLIDE DERIVATIVE; NATURAL PRODUCT;

ARTICLE; CANCER CELL; CANCER CELL CULTURE; CONTROLLED STUDY; HYDROPHILIC INTERACTION CHROMATOGRAPHY; LABORATORY; NONHUMAN; PRIORITY JOURNAL; PURIFICATION; REVERSED PHASE LIQUID CHROMATOGRAPHY; SCREENING; SKIN; STEREOISOMERISM; TOAD;

ANIMALS; BUFANOLIDES; BUFO BUFO; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, REVERSE-PHASE; HYDROPHOBICITY; SKIN;

ANURA; BUFO GARGARIZANS;

EID: 77952805399     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200900848     Document Type: Article

References (30)

1. Steyn, P. S., van Heerden, F. R., Nat. Prod. Rep. 1998, 15, 397-413.
2. Hashimoto, S., Jing, Y. K., Kawazoe, N., Masuda, Y., Nakajo, S., Yoshida, T., Kuroiwa, Y., Nakaya, K., Leuk. Res. 1997, 21, 875-883.
3. Taniguchi, M., Kubo, I., J. Nat. Prod. 1993, 56, 1539-1546.
4. Yamagishi, T., Haruna, M., Yan, X. Z., Chang, J. J., Lee, K. H., J. Nat. Prod. 1989, 52, 1071-1079.
5. Yeh, J. Y., Huang, W. J., Kan, S. F., Wang, P. S., Prostate 2003, 54, 112-124.
6. Dai, L. P., Gao, H. M., Wang, Z. M., Wang, W. H., Yao Xue Xue Bao 2007, 42, 858-861.
7. Cunha Filho, G. A., Schwartz, C. A., Resck, I. S., Murta, M. M., Lemos, S. S., Castro, M. S., Kyaw, C., PiresJr, O. R., Leite, J. R. S., BlochJr, C., Schwartz, E. F., Toxicon 2005, 45, 777-782.
8. Dinan, L., Harmatha, J., Lafont, R., J. Chromatogr. A 2001, 935, 105-123.
9. Okamoto, M., Chromatographia 1988, 26, 145-148.
10. Tittel, G., Wagner, H., Planta Med. 1980, 39, 125-134.
11. Krenn, L., Kopp, B., Phytochemistry 1998, 48, 1-29.
12. Abel, U., Koch, C., Speitling, M., Hansske, F. G., Curr. Opin. Chem. Biol. 2002, 6, 453-458.
13. Koehn, F. E., J. Med. Chem. 2008, 51, 2613-2617.
14. Eldridge, G. R., Vervoort, H. C., Lee, C. M., Cremin, P. A., Williams, C. T., Hart, S. M., Goering, M. G., O'Neil-Johnson, M., Zeng, L., Anal. Chem. 2002, 74, 3963-3971.
15. Liu, Y. M., Xue, X. Y., Guo, Z. M., Xu, Q., Zhang, F. F., Liang, X. M., J. Chromatogr. A 2008, 1208, 133-140.
16. Qiu, Y., Jiang, Y., Chen, J., He, J., Li, Z., SHANDONG GREEN TEA PHARM CO LTD (SHAN-Non-standard), p. 16.
17. Shimada, K., Ro, J. S., Ohishi, K., Nambara, T., Chem. Pharm. Bull. (Tokyo) 1985, 33, 2767-2771.
18. Yu, N., Xu, W., Jiang, Z. G., Cao, Q. H., Chu, Y. W., Xiong, S. D., Immunol. Lett. 2007, 114, 94-102.
19. Hou, L., Du, J., Wang, J., Liu, Y., Sun, W., Zheng, Y., Zhang, L., Hu, H., Dai, X., Guan, W., J. Cancer Res. Clin. Oncol. 2010. DOI 10.1007/s00432-00009-00724-z.
20. Guo, Z. M., Jin, Y., Liang, T., Liu, Y. F., Xu, Q., Liang, X. M., Lei, A. W., J. Chromatogr. A 2009, 1216, 257-263.
21. Ye, M., Guo, D. A., Rapid Commun. Mass Spectrom. 2005, 19, 1881-1892.
22. Gilar, M., Olivova, P., Daly, A. E., Gebler, J. C., Anal. Chem. 2005, 77, 6426-6434.
23. Jandera, P., J. Sep. Sci. 2008, 31, 1421-1437.
24. Kalili, K. M., de Villiers, A., J. Chromatogr. A 2009, 1216, 6274-6284.
25. Alpert, A. J., J. Chromatogr. 1990, 499, 177-196.
26. Zhao, Y. F., Luo, X. P., Ming, Y. F., Chen, L. R., Li, Y. M., J. Pharm. Biomed. Anal. 2006, 41, 124-128.
27. Kamano, Y., Kotake, A., Takano, R., Morita, H., Takeya, K., Itokawa, H., Heterocycles 1998, 49, 275-279.
28. Wang, J. D., Narui, T., Takatsuki, S., Hashimoto, T., Kobayashi, F., Ekimoto, H., Abuki, H., Niijima, K., Okuyama, T., Chem. Pharm. Bull. 1991, 39, 2135-2137.
29. Meinwald, J., Wiemer, D. F., Eisner, T., J. Am. Chem. Soc. 1979, 101, 3055-3060.
30. Kamano, Y., Nogawa, T., Yamashita, A., Pettit, G. R., Collect. Czech. Chem. Commun. 2001, 66, 1841-1848.