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Volumn 1, Issue 10, 2010, Pages 1616-1622

How the level of ordering of 2d nanocrystal superlattices is controlled by their deposition mode

Author keywords

[No Author keywords available]

Indexed keywords

CLASSICAL METHODS; COATING AGENTS; DECANETHIOL; DEPOSITION MODES; DODECANE; DODECANETHIOLS; DROPLET DEPOSITION; INTRINSIC PROPERTY; LONG-RANGE ORDERING; OXYGEN PLASMAS;

EID: 77952680384     PISSN: None     EISSN: 19487185     Source Type: Journal    
DOI: 10.1021/jz100417s     Document Type: Article
Times cited : (19)

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    • If we take into account the procedure used to disperse the nanocrystals in octane, decane, and dodecane (i.e., evaporation of the hexane from the mother solution and then dispersion in an other solvent), this could be attributed to the fact that some hexane molecules remain strongly adsorbed on the thiol chains. For any used coating agent, the nanocrystals previously dispersed in hexane are entirely dispersed in octane after hexane evaporation, while the amount of nanocrystals is rather low when dispersed in decane and dodecane. This indicates that the increase in the number of carbon atoms in the solvent hydrocarbon chain decreases the nanocrystals solubility, which is related to the fact that larger solvent molecules cannot easily penetrate into the coating chains' corona. The dispersion in the other solvents involves a competition between the hexane molecules already adsorbed and the adsorption of the new solvent molecules (octane, decane, or dodecane) coming from the bulk phase, leading to the replacement of some hexane ones. The affinity between the coating and solvent tails increases upon increasing the solvent length, which improves the thiol tails' organization and induces, therefore, a greater permeation of the soft coronas to reach a maximum. A further increase in the solvent length reduces the permeation due to the adsorption of larger solvent molecules on the thiol tails.
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