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Volumn 13, Issue 5, 2010, Pages 641-644

A 3D-diamond-like coordination network of lead(II) complex: Synthesis, structure and luminescent property

Author keywords

Coordination polymer; Diamond like network; Lead(II) complex; Luminescent property

Indexed keywords


EID: 77952106432     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.03.008     Document Type: Article
Times cited : (17)

References (51)
  • 23
    • 77952107954 scopus 로고    scopus 로고
    • Syntheses: the furan-2-ylmethylene salicyloyl hydrazone (H2fysh) was synthesized by a procedure, which is similar to that in reference [18, Synthesis of compound 1: Pb(NO3)2 (0.033 g, 0.10 mmol) was added to a solution of H2fysh ligand (0.027 g, 0.11 mmol) in a mixed solvent of methanol and DMF (5:1 v/v, 12 mL) with stirring. After stirring for 1 h, the suspension was filtered. The filtrate was left at room temperature about 4 months. Orange-red prism crystals suitable for X-ray diffraction were obtained by slow evaporation in 53% yield based on Pb(NO3)2. Anal. Calcd for C24H18N4O6Pb: C, 43.31; H, 2.73; N, 8.42, Found: C, 43.78; H, 2.59; N, 8.29
    • 6Pb: C, 43.31; H, 2.73; N, 8.42%. Found: C, 43.78; H, 2.59; N, 8.29%.
  • 24
    • 77952108030 scopus 로고    scopus 로고
    • 2=0.0524 for 2718 independent reflections. The diffraction data were collected on a Rigaku Weissenberg IP diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The structure was solved with direct methods and refined with full-matrix least-squares (SHELX-97).
    • 2=0.0524 for 2718 independent reflections. The diffraction data were collected on a Rigaku Weissenberg IP diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The structure was solved with direct methods and refined with full-matrix least-squares (SHELX-97).
  • 51
    • 77952105453 scopus 로고    scopus 로고
    • S.-X. Liu, M.-X. Xue, et al, a research work concerning several ligands and complexes, in progress
    • (f) S.-X. Liu, M.-X. Xue, et al., a research work concerning several ligands and complexes, in progress.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.