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Volumn 129, Issue 34, 2007, Pages 10334-10335

Anion control in the lonothermal synthesis of coordination polymers

Author keywords

[No Author keywords available]

Indexed keywords

ANION; COBALT DERIVATIVE; IONIC LIQUID; POLYMER;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; HYDROGEN BOND; HYDROPHOBICITY; SOLUBILITY; SYNTHESIS;

EID: 34548206737 PISSN: 00027863 EISSN: None Source Type: Journal
DOI: 10.1021/ja0737671 Document Type: Article

Times cited : (202)

References (17)

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14
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- Synthesis: for 1 Co(OAc)2·4H2O (380 mg, 1.5 mmol, Fisons, Trimesic acid (TMA-H3, 210 mg, 1 mmol, Avocado) and ∼10 mmol EMIm-Br were sealed and heated in a 23 mL Teflon-lined stainless steel autoclave at 150°C for 3 days. Dark-purple block crystals of 1 were collected with 75% yield. The similar method was followed for other compounds. For 2 Co(OAc)2·4H2O (1.5 mmol, TMA-H3 (1 mmol) and ∼5 mmol EMIm-Br and ∼5 mmol EMIm-Tf2N were mixed and heated at 150°C for 3 days. Purple plate crystals were collected with 65% yield. Some samples of 2 contain a small amount of Li+ impurity that is present in the EMIM-Tf 2N starting material. For 3 Co(OAc)2·4H 2O (1.5 mmol, TMA-H3 (1 mmol) and ∼10 mmol EMIm-Tf2N were mixed and heated at 110°C for 5 days. A mixture of orange bar
- 2N were mixed and heated at 150°C for 3 days. Orange plate crystals were collected with total 60% yield.

15
- 34548205875
- Crystal data for 1: T, 90(2) K, λ, 0.67130 Å, orthorhombic, Pbca, a, 14.2616(4) Å, b, 16.1525(5) Å, c, 16.4867(5) Å, V, 3797.9(2) Å3, Z, 4, Dcalcd, 1.629 Mg/m 3, μ, 1.373 mm-1, 2θ, 2.98 to 26.99°, data/restraints/parameters, 4883/0/251, GOF, 1.098, R1, 0.0454, wR2(all, 0.1328. Crystal data for 2: T, 113(2) K, λ, 0.71073 Å, orthorhombic, Pbca, a, 15.425(2) Å, b, 12.184(2) Å, c, 16.059(2) Å, V, 3018.1(7) Å3, Z, 8, Dc, 1.558 Mg/m3, μ, 0.800 mm-1, 2θ, 2.48 to 26.00°, data/restraints/parameters, 2828/0/235, GOF, 1.198, R 1, 0.0882, wR2all, 0.2199. Crystal data for 3: T, 113
- + cations in 1 and 4.

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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.