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Volumn 13, Issue 5, 2010, Pages 645-648

Synthesis, structures and properties of Cu and Cd complexes with 1,10-phenanthroline

Author keywords

1, 10 phenanthroline; crystals structure; fluorescence; weak interactions

Indexed keywords


EID: 77952100786     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2010.03.009     Document Type: Article
Times cited : (17)

References (43)
  • 31
    • 77952102328 scopus 로고    scopus 로고
    • Synthesis of [Cu(phen)(isca)(EtOH, 1, To a solution of phen (0.180 g, 1mmol) in EtOH (10mL) was slowly added to a solution of CuCl2 (0.132 g, 1mmol) in deionized water (10 mL, The mixture was stirred for 10 min at room temperature and then placed in a 25 mL Teflon-lined autoclave and heated at 80°C for 120 h. The autoclave was cooled over a period of 5 h at 10 °Ch-1, and the product was collected by filtration, then dried at ambient temperature to give 1 as blue crystals. Yield: (75, based on Cu, Anal. Calcd for C22H18CuN2O5, C, 58.21; H, 4.00; N, 6.17. Found: C, 58.96; H, 4.15; N, 6.56. IR data (KBr pellets, cm-1, 2950w (v CH3, 3350s (v H-O, 1690, 1556m v C, N, 1363, 1160, 1080, 852, 760, 563
    • 3), 3350s (v H-O), 1690, 1556m (v C = N), 1363, 1160, 1080, 852, 760, 563.
  • 32
    • 77952102775 scopus 로고    scopus 로고
    • -1): 1731s (v C = O), 1565m (v C = N), 1520, 1307s, 1100s (v Cl=O), 849, 772, 726, 627, 427.
    • -1): 1731s (v C = O), 1565m (v C = N), 1520, 1307s, 1100s (v Cl=O), 849, 772, 726, 627, 427.
  • 33
    • 77952101071 scopus 로고    scopus 로고
    • -1): 1565m (v C = N), 1520, 1305s, 849s.
    • -1): 1565m (v C = N), 1520, 1305s, 849s.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.