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note
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Crystallographic data for compound 5a have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 752077. Copies of the data can be obtained, free of charge, on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK. Fax: +44 1223-336033. E-mail: deposit@ccdc.cam.ac.uk.
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79
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77949540696
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note
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Generally, in epoxides, the trans-vicinal coupling is small as compared to the cis-vicinal coupling constant.
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80
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note
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1H NMR; wherein region at δ 5.8-6.1 was expanded and the ratio calculated for the H-1 by integration.
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84
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20144382745
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77949542266
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note
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G. M. Sheldrick, shelx-97 Program for Crystal Structure Solution and Refinement; University of Gottingen: Germany, 1997.
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