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Crystal data for 1a: C36H26N4O, Mr, 530.61, Orthorhombic, P n a 21. Crystal size: 0.4 × 0.25 × 0.2 mm3, a, 10.841(2) Å, b, 10.504(2) Å, c, 28.378(5) Å, α, 90°, β, 90°, γ, 90°, V, 3231.5(10) Å3, Z, 4, T, 301(2) K, ρcalcd, 1.091 g cm-3, μMo, 0.067 mm-1, F(000, 1112, total number of unique reflections 2539 (Rint, 0.0502, Numbers of parameters, 310, R1, 0.0997 and wR2, 0.2683. Crystallographic data (excluding structure factors) for 1a have been deposited with the Cambridge Crystallographic Data Center as supplementary publication nos. CCDC: 602983. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax:, 44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk
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2 = 0.2683. Crystallographic data (excluding structure factors) for 1a have been deposited with the Cambridge Crystallographic Data Center as supplementary publication nos. CCDC: 602983. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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