HPLC method for determination of fluorescence derivatives of cortisol, cortisone and their tetrahydro- and allo-tetrahydro-metabolites in biological fluids

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 878, Issue 3-4, 2010, Pages 283-289

  Główka, Franciszek K ^a   Kosicka, Katarzyna ^a   Karaźniewicz Łada, Marta ^a  

^a POZNAN UNIVERSITY OF MEDICAL SCIENCES   (Poland)

Author keywords

11 Hydroxysteroid dehydrogenase; 9 Anthroyl nitrile derivatization; Enzymatic hydrolysis; Urinary free cortisol; Urinary free cortisone

Indexed keywords

9-ANTHROYL NITRILE DERIVATIZATION; ANALYTES; BIOLOGICAL FLUIDS; CALIBRATION CURVES; CHROMATOGRAPHIC SEPARATIONS; DERIVATIZATION OF; DERIVATIZATIONS; GLUCOCORTICOIDS; GLUCURONIDASE; HPLC METHOD; HPLC-FLD; HYDROXYSTEROID DEHYDROGENASE; INTERNAL STANDARDS; ISOFORMS; MONOLITHIC COLUMNS; ORGANIC BASIS; PLASMA LEVELS; PREDNISOLONE; QUANTITATIVE DETERMINATIONS; QUINUCLIDINES; TRIETHYLAMINES;

BIOMOLECULES; BODY FLUIDS; CYANIDES; DICHLOROMETHANE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIPIDS; METABOLISM; METABOLITES;

ENZYMATIC HYDROLYSIS;

11BETA HYDROXYSTEROID DEHYDROGENASE ISOFORM 2; 9 ANTHROYL NITRILE; CORTISONE; DICHLOROMETHANE; GLUCOCORTICOID; HYDROCORTISONE; HYDROXYSTEROID DEHYDROGENASE; NITRILE; PREDNISOLONE; QUINUCLIDINE; TRIETHYLAMINE; UNCLASSIFIED DRUG;

ARTICLE; ENZYME ACTIVITY; FLUORESCENCE; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PH MEASUREMENT; PRIORITY JOURNAL;

BODY FLUIDS; BUFFERS; CALIBRATION; CHROMATOGRAPHY, GAS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CORTISONE; FLUORESCENCE; GLUCURONIDASE; HUMANS; HYDROCORTISONE; HYDROLYSIS; LIMIT OF DETECTION; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; TEMPERATURE; TETRAHYDROCORTISOL; TETRAHYDROCORTISONE; TIME FACTORS;

EID: 74049083807     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2009.11.016     Document Type: Article

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