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The crystal data of 2e have been deposited in CCDC with number 732287. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax +44-1223/336-033; E-mail deposit@ccdc.cam.ac.uk, Empirical formula C28H26O 3; formula weight 410.49; crystal size 0.217 x 0.216 x 0.041; crystal color colorless, crystal habit prismatic; crystal system monoclinic; lattice type primitive; lattice parameters a, 13.5410(18) Å, b, 16.611(2) Å, c, 10.4723(14) Å, α, 90°, β, 108.179(3)°, γ, 90°, V, 2237.9(5) Å3; space group P2(1)/c; Z, 4; Dcalc, 1.218 g/cm3; F000, 872; R1, 0.0474, wR2, 0.0913; diffractometer Rigaku AFC7R
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2 = 0.0913; diffractometer Rigaku AFC7R.
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33
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73149116975
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The crystal data of 3a have been deposited in CCDC with number 704726. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (Fax +44-1223/336-033; E-mail deposit@ccdc.cam.ac.uk, Empirical formula C27H24O 2; formula weight 380.46; crystal size 0.412 x 0.201 x 0.075; crystal color colorless, crystal habit prismatic; crystal system orthorhombic; lattice type primitive; lattice parameters a, 11.3164(12) Å, b, 17.6548(19) Å, c, 20.537(2) Å, α, 90°, β, 90°, γ, 90°, V, 4103.0(8) Å3; space group Pcab; Z, 8; Dcalc, 1.232 g/cm3; F000, 1616; R1, 0.0777, wR 2, 0.1888; diffractometer Rigaku AFC7R
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2 = 0.1888; diffractometer Rigaku AFC7R.
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