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72949094310
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Crystal data for 1: Formula C28H32Cu 2N2O9 fw, 667.66, triclinic, P1̄ (No. 2, a, 8.5387(2) Å, b, 9.2448(3) Å, c, 10.4427(3) Å; α, 111.759(2)°; β, 96.228(2)°; γ, 100.746(2)°; V= 737.79(4)Å3, Z, 1; P calcd, 1.503 g cm-3 μ(MoKa, 1.496 mm -1, F(000, 344, T, 298 K, λ (MOka, 0.71073 Å, θmax, 27.9°, total data, 14 922, unique data, 3466, Rint, 0.091, observed data [I > 2aI, 2162, R, 0.0605, Rw, 0.1673, GOF, 1.01
-
w = 0.1673, GOF = 1.01.
-
-
-
-
41
-
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72949084930
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Cell parameters for 1′: a, 13.292(13) Å, b, 9.245(10, Å c, 10.345(13) Å, α, 111.57(12)°, β, 96.67(10)°, γ, 91.85(11)°; V= 1170.32 Å3
-
3.
-
-
-
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42
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72949117537
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The size is measured by considering van der Waals radii for the constituting atoms
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(a) The size is measured by considering van der Waals radii for the constituting atoms
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-
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44
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0032503514
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Webster, C. E.; Drago, R. S.; Zerner, M., C. J. Am. Chem. Soc. 1998, 120, 5509.
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Webster, C. E.; Drago, R. S.; Zerner, M., C. J. Am. Chem. Soc. 1998, 120, 5509.
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