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Angewandte Chemie - International Edition

Volumn 48, Issue 30, 2009, Pages 5513-5516

Direct synthesis of iron, cobalt, nickel, and copper complexes of n-heterocyclic carbenes by using commercially available metal powders

(3) Liu, Bin a Xia, Qinqin a Chen, Wanzhi a

a ZHEJIANG UNIVERSITY (China)

Author keywords

Cobalt; Copper; Iron; N heterocyclic carbenes; Nickel

Indexed keywords

CARBENE COMPLEXES; COPPER COMPLEXES; DIRECT SYNTHESIS; GOOD YIELD; IMIDAZOLIUM SALT; METAL POWDER; MIXED-VALENT; N-HETEROCYCLIC CARBENES; SYNTHETIC METHODS;

COBALT; COPPER; COPPER COMPOUNDS; IONIC LIQUIDS; IRON COMPOUNDS; METAL COMPLEXES; NICKEL; NICKEL ALLOYS; POWDER METALLURGY; POWDER METALS; SILVER;

COBALT COMPOUNDS;

EID: 70349917640 PISSN: 14337851 EISSN: None Source Type: Journal
DOI: 10.1002/anie.200901850 Document Type: Article

Times cited : (147)

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- Crystal data for 1: C17H14F12FeN 6P2, monoclinic, C2/c, a, 16.579 (2, b, 11.5559 (12, c, 14.0775 (19) Å, β= 124.855 (2) °, V= 2213.3 (5) Å3, Z, 4, ρcalcd, 1.945 Mgm-3, 5672 reflections collected, 1947 reflections independent [Rint, 0.0390, GOF on F2 1.031, R [I>2σI, 0.0688, 0.1765; 2: C17H14CoF 12N6P2, monoclinic, C2/c, a, 16.5720 (19, b, 11.5538 (11, c, 14.0741 (13) Å, β, 124.829 (2) °, V= 2212.0 (4) Å3, Z, 4, ρcalcd, 1.959 Mgm-3, 5612 reflections collected, 1946 reflections independent [Rint, 0.0237, GOF on F 2 1.066, R [1&2σI, 0.0379, 0.0983; 4: C68H
- 2 1.067, R [I>2σI]: 0.0588, 0.1595. CCDC 726608-726615 (1, 2, 4-9) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Crystallographic Data Centre via www.ccdc.cam.uk/data request/cif.

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