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The already high yield of the reaction can be further improved from 83 % to 90 % by scaling up the literature procedure by a factor of 20. In addition, while the authors of reference [12] stated that noria was precipitated as a white solid, using this method we consistently isolated a light yellow powder that, from analysis, was found to be pure 1.
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16] CCDC 717929 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data-request/cif.
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For this approximate calculation, dummy atoms were placed at entrances to the molecular cavity prior to calculation of internal
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