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Volumn 7, Issue 17, 2009, Pages 3385-3387

Tandem SmI2-induced nitrone β-elimination/aldol-type reaction

Author keywords

[No Author keywords available]

Indexed keywords

KETONES;

EID: 70349299895     PISSN: 14770520     EISSN: None     Source Type: Journal    
DOI: 10.1039/b910486k     Document Type: Article
Times cited : (8)

References (37)
  • 32
    • 41749108394 scopus 로고    scopus 로고
    • 2 are needed to complete the reaction. In addition, benzyl alcohol was produced (from NMR analysis of the crude reaction mixture) See ESI for ESI-MS and NMR data
    • I. M. Rudkin L. C. Miller D. J. Procter Organomet. Chem. 2008 34 19
    • (2008) Organomet. Chem. , vol.34 , pp. 19
    • Rudkin, I.M.1    Miller, L.C.2    Procter, D.J.3
  • 35
    • 0037122183 scopus 로고    scopus 로고
    • Typical procedure: see ESI For reproducible results, co-evaporation of the starting nitrone several times with toluene, use of THF dried over molecular sieves, and thorough purge of the reaction media using Schlenk techniques were essential. Addition of proton sponge to the reaction mixtures did not improve the yields in alkylation products For a general review on the chemistry of nitrones see:
    • A. Bøgevig K. V. Gothelf K. A. Jørgensen Chem.-Eur. J. 2002 8 5652
    • (2002) Chem.-Eur. J. , vol.8 , pp. 5652
    • Bøgevig, A.1    Gothelf, K.V.2    Jørgensen, K.A.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.