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69449084277
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Using 1.5 equiv of bromoallene gave product 5 in 76% yield
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Using 1.5 equiv of bromoallene gave product 5 in 76% yield.
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50
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69449098215
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-
3N) resulted in isomerized product. Chromatography on basic alumina (pH = 9.5) was therefore chosen
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3N) resulted in isomerized product. Chromatography on basic alumina (pH = 9.5) was therefore chosen.
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51
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69449099808
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No product formation was observed when the copper catalyst was removed from the system
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No product formation was observed when the copper catalyst was removed from the system.
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52
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69449094626
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And 2 equiv of p-benzoquinone in THF at 55°C afforded the the pyrroline product 1-tosyl-3-(2-isopropenyl4-vinyl-2-pyrroline) in 89% yield: Persson, A. K. Å
-
2
-
2 and 2 equiv of p-benzoquinone in THF at 55°C afforded the the pyrroline product (1-tosyl-3-(2-isopropenyl4-vinyl- 2-pyrroline) in 89% yield: Persson, A. K. Å; Bäckvall, J. E. Unpublished results.
-
Bäckvall, J. E. Unpublished Results.
-
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