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Crystallographic measurements were made at 100.0(1) using a Bruker Apex2 CCD diffractometer with a graphite monochromated Mo Ka radiation at a detector distance of 5 cm and with APEX2 software. The collected data were reduced using SAINT program, and the empirical absorption corrections were performed using SADABS program, Bruker. APEX2 Version 1.27, SAINT and SADABS; Bruker AXS: Madison, WI, USA, 2005, The structures were solved by direct methods and refined by least-squares using the SHELXTL software package [Sheldrick, G. M. SHELXTL Version 5.1; Bruker AXS: Madi-son, WI, USA, 1998, Crystal, data 1: C80H56Br6N16Pb3, M r, 2342.41, Orthorhombic, Fddd, a, 34.5177(4, b, 7.23000(1.0, c, 58.8102(6) Å, V, 14676.8(3) Å3, Z, 8, pc, 2.120 Mg-cm-3, Mo-Kα, radiation λ, 0.71073 Å, graphite monochromator, crystal size 0.20 × 0.09
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