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Crystal data 1: C18H20N2O4, Mr, 535.55, monoclinic, C2, a, 9.8306(11, b, 5.8877(6, c, 15.5039(17) Å, a, 90.00°, β, 104.7320(10)°, γ, 90.00°, V, 867.76(16) Å3, Z, 2, ρo, 2.049 Mg cm-3, MoKα radiation (λ, 0.71073 Å, graphite monochromator, crystal size 0.24 × 0.21 × 0.20 mm3, T, 100(2) K, 2.72° ≤ θ ≤ 26.68°, 12 ≤ h ≤ 12, 7 ≤ k ≤ 7, 19 ≤ 1 ≤ 19, 4437 reflections measured of which 1895 were symmetrically independent (1881 reflections with I > 2σ(I, Rint, 0.0341, 114 parameters, 1 restraints, R(F, 0.0280 (I > 2σ(I, wR(F2, 0.0699 all data, S, 0.993
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2) = 0.0699 (all data), S = 0.993.
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