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Volumn 28, Issue 15, 2009, Pages 4258-4261

Synthesis of [{2,6-(Me2NCH2)2C 6H3}Sn(OH)0]6: An N-Sn coordinated stannonic acid

Author keywords

[No Author keywords available]

Indexed keywords

CENTROSYMMETRIC; MONOORGANOTIN; PINCER LIGANDS;

EID: 68149182583     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om9002889     Document Type: Article
Times cited : (20)

References (33)
  • 14
    • 0004063249 scopus 로고    scopus 로고
    • 2nd ed, Wiley-VCH: Weinheim, Germany
    • (c) Davies, A. G. Organotin Chemistry, 2nd ed., Wiley-VCH: Weinheim, Germany, 2004.
    • (2004) Organotin Chemistry
    • Davies, A.G.1
  • 29
    • 68149137005 scopus 로고    scopus 로고
    • 14
    • 14
  • 30
    • 68149141787 scopus 로고    scopus 로고
    • Crystal data for 3-KO2CCF3 are as foljows: monoclinic, space group C2/C, a, 26.8747(5) A, b, 16.0436(6) A, c, 25.7439(4) A, β, 115.888(12)°, K= 9986.4(1) À3, p =1.577 g cm-3, Z, 4. Final* indices (I > 2a(I, Rl, 0.044, wR2, 0.108. The structure was solved by direct methods (SIR92)13 and refined by a full-matrix least-squares procedure based on F2 (SHELXL97).14 There are disordered solvents (THF, CH 2Cl2) and a CF3CO2 anion in this structure. Attempts were made to model this disorder or split it into two or more positions, but these were unsuccessful. PLATON/SQUEEZE15 was used to correct the data for the presence of disordered solvent
    • 15 was used to correct the data for the presence of disordered solvent.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.