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Crystal data for 3-KO2CCF3 are as foljows: monoclinic, space group C2/C, a, 26.8747(5) A, b, 16.0436(6) A, c, 25.7439(4) A, β, 115.888(12)°, K= 9986.4(1) À3, p =1.577 g cm-3, Z, 4. Final* indices (I > 2a(I, Rl, 0.044, wR2, 0.108. The structure was solved by direct methods (SIR92)13 and refined by a full-matrix least-squares procedure based on F2 (SHELXL97).14 There are disordered solvents (THF, CH 2Cl2) and a CF3CO2 anion in this structure. Attempts were made to model this disorder or split it into two or more positions, but these were unsuccessful. PLATON/SQUEEZE15 was used to correct the data for the presence of disordered solvent
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15 was used to correct the data for the presence of disordered solvent.
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Camalli, M.7
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