Reaction of butyltin hydroxide oxide with p-toluenesulfonic acid: Synthesis, X-ray crystal analysis, and multinuclear NMR characterization of {(BuSn)12O14(OH)6}(4-CH3C 6H4SO3)2

Organometallics

Volumn 19, Issue 10, 2000, Pages 1940-1949

  Eychenne Baron, Christophe ^a   Ribot, François ^a   Steunou, Nathalie ^a   Sanchez, Clément ^a   Fayon, Franck ^b   Biesemans, Monique ^c   Martins, José C ^c   Willem, Rudolph ^c  

^a UNIVERSITÉ PIERRE ET MARIE CURIE   (France)

^b Centre National de la Recherche Scientifique   (France)

^c VRIJE UNIVERSITEIT BRUSSEL   (Belgium)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0000493055     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om990877a     Document Type: Article

References (46)

1. Ribot, F.; Eychenne-Baron, C.; Sanchez, C. Phosphorus, Sulfur Silicon Relat. Elem. 1999, 150-151, 41.
2. Chandrasekhar, V.; Day, R. O.; Holmes, R. R. Inorg. Chem. 1985, 24, 1970.
3. Day, R. O.; Holmes, J. M.; Chandrasekhar, V.; Holmes, R. R. J. Am. Chem. Soc. 1987, 109, 940.
4. Day, R. O.; Chandrasekhar, V.; Kumara Swamy, K. C.; Holmes, J. M.; Burton, S. D.; Holmes, R. R. Inorg. Chem. 1988, 27, 2887.
5. Holmes, R. R. Acc. Chem. Res. 1989, 22, 190.
6. Puff, H.; Reuter, H. J. Organomet. Chem. 1989, 368, 173.
7. Puff, H.; Reuter, H. J. Organomet. Chem. 1989, 373, 173.
8. Dakternieks, D.; Zhu, H.; Tiekink, E. R. T.; Colton, R. J. J. Organomet. Chem. 1994, 476, 33.
9. Banse, F.; Ribot, F.; Tolédano, P.; Maquet, J.; Sanchez, C. Inorg. Chem. 1995, 34, 6371.
10. Jaumier, P.; Jousseaume, B.; Lahcini, M.; Ribot, F.; Sanchez, C. J. Chem. Soc., Chem. Commun. 1998, 369.
11. Eychenne-Baron, C.; Ribot, F.; Sanchez, C. J. Organomet. Chem. 1998, 567, 137.
12. McCarthy, G.; Welton, J. Powder Diffr. 1989, 4, 156.
13. Blunden, S. J.; Hill, R.; Suton, S. E. Appl. Organomet. Chem. 1991, 5, 159.
14. Haus, E.; Sebald, A. Magn. Reson. Chem. 1994, 32, 679.
15. Harris, R. K.; Lawrence, S. E.; Oh, S. W. J. Mol. Struct. 1995, 347, 309.
16. Ribot, F.; Sanchez, C.; Meddour, A.; Gielen, M.; Tiekink, E. R. T.; Biesemans, M.; Willem, R. J. Organomet. Chem. 1998, 552, 177.
17. Ribot, F.; Sanchez, C.; Willem, R.; Martins, J. C.; Biesemans, M. Inorg. Chem. 1998, 37, 911.
18. Ribot, F.; Banse, F.; Diter, F.; Sanchez, C. New J. Chem. 1995, 19, 1145.
19. Willem, R.; Bouhdid, A.; Kayser, F.; Delmotte, A.; Gielen, M.; Martins, J. C.; Biesemans, M.; Tiekink, E. R. T., Organometallics 1996, 15, 1920.
20. (a) Neuhaus, D.; Williamson, M. P. The Nuclear Overhauser Effect in Structural and Conformational Analysis; VCH: New York, 1989.
21. (b) Cavanagh, J.; Fairbrother, W. J.; Palmer, A. G., III; Skelton, N. J. Protein NMR Spectroscopy Principles and Practice; Academic Press: San Diego, CA, 1996.
22. (a) Bothner-By, A. A.; Stephens, R. L.; Lee, J.-M.; Warren, C. D.; Jeanloz, R. W. J. Am. Chem. Soc. 1984, 106, 811.
23. (b) Bax, A.; Davis, D. G. J. Magn. Reson. 1985, 63, 207.
24. The ortho-meta H-H distance was determined from a phenyl moiety available in the Insight II builder fragment library (Insight II, 95.0, MSI Scranton Road, San Diego, CA).
25. anion) to be calculated at 2.5 Å.
26. Willker, W.; Leibfritz, D. Magn. Reson. Chem. 1995, 33, 632.
27. Martins, J. C.; Biesemans, M.; Willem, R. Prog. NMR Spectrosc., in press.
28. (a) Massiot, D.; Farnan, I.; Gautier, N.; Trumeau, D.; Trokiner, A.; Coutures, J.-P. Solid State NMR 1995, 4, 241.
29. (b) Fayon, F.; Bessada, C.; Massiot, D.; Farnan, I.; Coutures, J.-P. J. Non-Cryst. Solids 1998, 232-234, 403.
30. The use of anhydrous dioxane (less 0.1% of water) resulted in an incomplete crystallization, as evidenced by lower yields. The use of dioxane with 1% of water resulted in a faster, but unclean, crystallization. Therefore, dioxane with 0.5% of water was preferred for crystallizing 1-diox.
31. Walker, N.; Stuart, D. Acta Crystallogr., Sect. A 1983, 39, 158.
32. Sheldrick, G. M. SHELXS-86, Program for Automatic Solution of Crystal Structure; University of Göttingen, Göttingen, Germany, 1986.
33. Watkin, D. J.; Prout, C. K.; Carruthers, J. R.; Betteridge, P. W. CRYSTALS issue 10; Chemical Crystallography Laboratory, University of Oxford, Oxford, U.K., 1996.
34. Watkin, D. J.; Prout, C. K.; Pearce, L. J.; CAMERON; Chemical Crystallography Laboratory, University of Oxford, Oxford, U.K., 1996.
35. Reuter, H.; Sebald, A. Z. Naturforsch. 1992, 48B, 195.
36. Massiot, D.; Thiele, H.; Germanus, A. Bruker Rep. 1994, 140, 43.
37. Herzfeld, J.; Berger, A. E. J. Chem. Phys. 1980, 73, 6021.
38. Haeberlen, U. Adv. Magn. Reson. 1976, Suppl. 1.
39. Bax, A.; Griffey, R. H.; Hawkins, B. L. J. Magn. Reson. 1983, 55, 301.
40. (a) Keeler, J.; Clowes, R. T.; Davis, A. L.; Laue, E. D. Methods Enzymol. 1994, 239, 145.
41. (b) Tyburn, J.-M.; Bereton, I. M.; Doddrell, D. M. J. Magn. Reson. 1992, 97, 305.
42. (c) Ruiz-Cabello, J.; Vuister, G. W.; Moonen, C. T. W.; Van Gelderen, P.; Cohen, J. S.; Van Zijl, P. C. M. J. Magn. Reson. 1992, 100, 282.
43. (d) Vuister, G. W.; Boelens, R.; Kaptein, R.; Hurd, R. E.; John, B. K.; Van Zijl, P. C. M. J. Am. Chem. Soc. 1991, 113, 9688.
44. (a) Kayser, F.; Biesemans, M.; Gielen, M.; Willem, R. J. Magn. Reson. 1993, A102, 249.
45. (b) Martins, J. C.; Kayser, F.; Verheyden, P.; Gielen, M.; Willem, R.; Biesemans, M. J. Magn. Reson. 1997, 124, 128.
46. (c) Kayser, F.; Biesemans, M.; Gielen, M.; Willem, R. In Advanced Applications of NMR to Organometallic Chemistry; Gielen, M., Willem, R., Wrackmeyer, B., Eds.; Wiley: Chichester, U.K., 1996; Chapter 3, pp 45-86.