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0342633300
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note
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3): δ = - 486.6 (s).
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24
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0343503475
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note
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3. Three of the n-butyl groups are disordered and each is modeled in two orientations. Three solvent sites are found in the regions of the disordered butyl groups, which are also disordered. A fourth disordered solvent site is located away from the main species and is modeled in three orientations. Restraints were applied to the positional and displacement parameters of the disordered atoms. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-137558. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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25
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Weber, B.9
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26
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0030896332
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0343939330
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note
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0004283942
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0003872738
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