Formation of a thermally stable, porous coordination network via a crystalline-to-amorphous-to-crystalline phase transition

Journal of the American Chemical Society

Volumn 131, Issue 11, 2009, Pages 3860-3861

  Ohara, Kazuaki ^a   Martí Rujas, Javier ^a   Haneda, Tsuyoshi ^a   Kawano, Masaki ^a   Hashizume, Daisuke ^b   Izumi, Fujio ^c   Fujita, Makoto ^a  

^a UNIVERSITY OF TOKYO   (Japan)

^b RIKEN   (Japan)

^c NATIONAL INSTITUTE FOR MATERIALS SCIENCE   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

AB INITIO; AROMATIC SOLVENT; COORDINATION NETWORKS; CRYSTALLINE PHASE TRANSITION; CRYSTALLINE-TO-AMORPHOUS; GUEST MOLECULES; POROUS STRUCTURES; POWDER X RAY DIFFRACTION; SOLID-STATE PHASE TRANSITION; THERMALLY STABLE;

CRYSTAL STRUCTURE; CRYSTALLINE MATERIALS; ORGANIC SOLVENTS;

PHASE TRANSITIONS;

ZEOLITE; ZINC COMPLEX;

ARTICLE; CHEMICAL STRUCTURE; COMPLEX FORMATION; CRYSTAL; CRYSTAL STRUCTURE; CRYSTALLIZATION; DIFFERENTIAL SCANNING CALORIMETRY; MATERIALS; MOLECULE; PHASE TRANSITION; PHYSICAL PHASE; TEMPERATURE; THERMOSTABILITY; X RAY CRYSTALLOGRAPHY; X RAY DIFFRACTION;

EID: 67849114561     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9005145     Document Type: Article

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28. A high-quality PXRD pattern of phase III was recorded at 623 K in transmission mode (0.3 mm capillary; synchrotron radiation, λ = 0.9948 Å 2ø range, 2-70°; step size, 0.01°; data collection time, 20 min) on a diffractometer equipped with a blue-IP detector at the SPring-8 BL19B2 beam line.
29. 2 as an included guest was successfully determined by PXRD and will be reported elsewhere.