1H HR/MAS NMR in the suspended state: Molecular recognition processes in liquid chromatography between steroids and a silica hydride-based cholesterol phase

Journal of Separation Science

Volumn 32, Issue 10, 2009, Pages 1722-1728

  Friebolin, Volker ^a   Bayer, Marc P ^a   Matyska, Maria T ^b   Pesek, Joseph J ^b   Albert, Klaus ^a  

^a UNIVERSITY OF TÜBINGEN   (Germany)

^b SAN JOSE STATE UNIVERSITY   (United States)

Author keywords

1H HR MAS NMR spectroscopy in the suspended state; Cholesterol based stationary phase; HPLC; Hydrosilation; Molecular recognition process

Indexed keywords

1H HR/MAS NMR SPECTROSCOPY IN THE SUSPENDED STATE; ANGLE SPINNING; CHROMATOGRAPHIC DATA; COLUMN MATERIALS; HPLC; HYDROPHOBIC BINDING; HYDROSILATION; NMR SPECTROSCOPY; RETENTION TIME; SATURATION-TRANSFER DIFFERENCES; SEPARATION PROCESS; SILICA HYDRIDE; STATIONARY PHASE; STATIONARY PHASE MATERIALS;

BINDING ENERGY; CHOLESTEROL; CHROMATOGRAPHIC ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH PRESSURE LIQUID CHROMATOGRAPHY; HYDROSILYLATION; LIPIDS; MOLECULAR BIOLOGY; MOLECULAR RECOGNITION; NUCLEAR MAGNETIC RESONANCE; SILICA;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

CHOLESTEROL; CORTICOSTERONE; DEOXYCORTICOSTERONE ACETATE; HYDROXYPROGESTERONE; MEGESTROL ACETATE; METHYLPREDNISOLONE; PREDNISOLONE; PREDNISOLONE ACETATE; PROGESTERONE; SILICON DIOXIDE; STEROID; CHOLESTEROL ESTER; CHOLESTERYL 10 UNDECENOATE; CHOLESTERYL-10-UNDECENOATE; PROTON; SILICA HYDRIDE; SILICATE;

ARTICLE; BINDING AFFINITY; DRUG STRUCTURE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HIGH RESOLUTION MAGIC ANGLE SPINNING NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; HYDROPHOBICITY; MOLECULAR RECOGNITION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; PROCESS TECHNOLOGY; SEPARATION TECHNIQUE; STATIONARY PHASE; CHEMISTRY; CONFORMATION; ISOLATION AND PURIFICATION; METHODOLOGY; STANDARD; STEREOISOMERISM;

CHOLESTEROL; CHOLESTEROL ESTERS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR CONFORMATION; PROTONS; REFERENCE STANDARDS; SILICATES; STEREOISOMERISM; STEROIDS;

EID: 67649960991     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200800697     Document Type: Article

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