A comparison of NMR spectra obtained for solid-phase-synthesis resins using conventional high-resolution, magic-angle-spinning, and high-resolution magic-angle-spinning probes

Journal of Magnetic Resonance - Series A

Volumn 119, Issue 1, 1996, Pages 65-75

  Keifer, Paul A ^a   Baltusis, Laima ^a   Rice, David M ^a   Tymiak, Adrienne A ^b   Shoolery, James N ^c  

^a Varian Inc   (United States)

^b BRISTOL MYERS SQUIBB PHARMACEUTICAL RESEARCH INSTITUTE   (United States)

^c NMR Consultant   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0002108435     PISSN: 10641858     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmra.1996.0052     Document Type: Article

References (47)

1. P. Lloyd-Williams, R. Albericio, and E. Giralt, Tetrahedron 49, 11065-11133 (1993)
2. S. L. Beaucage and R. P. Iyer, Tetrahedron 48, 2223-2311, (1992).
3. A. Malik, H. Bauer, J. Tschakert, and W. Voelter, Chem.-Ztg. 114, 371-375 (1990).
4. B. A. Bunin, M. J. Plunkett, and J. A. Ellman, Proc. Natl. Acad. Sci. USA 91, 4708-4712 (1994).
5. R. Epton (Ed.), "Innovation and Perspectives in Solid Phase Synthesis - Peptides, Proteins, and Nucleic Acids," Mayflower Worldwide, Kingswinford, UK, 1994.
6. J. T. Randolph, K. F. McClure, and S. J. Danishefsky, J. Am. Chem. Soc. 117, 5712-5719 (1995).
7. H. Wenschuh, M. Beyermann, H. Haber, J. K. Seydel, E. Krause, M. Bienert, L. A. Carpino, A. El-Faham, and F. Albericio, J. Org. Chem. 60, 405-410 (1995).
8. A. M. Bray, R. M. Valerio, A. J. Dipasquale, J. Grieg, and N. J. Maeji, J. Pept. Sci. 1, 80-87 (1995).
9. D. Madden, V. Krchnák, and Michal Lebl, Perspect. Drug. Discovery Des. 2, 269 (1994).
10. J. J. Baldwin, J. J. Burbaum, I. Henderson, and M. H. J. Ohlmeyer, J. Am. Chem. Soc. 117, 5588-5589 (1995).
11. J. M. J. Fréchet, Tetrahedron 37, 663-683 (1981).
12. D. Doskocilová, B. Schneider, and J. Jakes, J. Magn. Reson. 29, 79-90 (1978).
13. H. D. H. Stöver and J. M. J. Fréchet, Macromolecules 24, 883-888 (1991).
14. S. Ganapathy, P. R. Rajamohanan, P. M. Ramanujulu, A. B. Mandhare, and R. A. Mashelkar, Polymers 35, 888-891 (1994).
15. W. L. Fitch, G. Detre, C. P. Holmes, J. N. Shoolery, and P. A. Keifer, J. Org. Chem. 59, 7955-7956 (1994).
16. R. C. Anderson, M. A. Jarema, M. J. Shapiro, J. P. Stokes, and M. Ziliox, J. Org. Chem. 60, 2650-2651 (1995).
17. N. C. Nielsen, R. Sangill, H. Bildsoe, and H. J. Jakobsen, Macromolecules 28, 2009-2015 (1995).
18. F. I. Auzanneau, M. Meldal, and K. Bock, J. Peptide Sci. 1, 31-44 (1995).
19. M. D. Swerdloff, S. B. Anderson, R. D. Sedgwick, M. K. Gabriel, R. J. Brambilla, D. M. Hindenlang, and J. I. Williams, Int. J. Pept. Protein Res. 33, 318-327 (1989).
20. G. C. Look, C. P. Holmes, J. P. Chinn, and M. A. Gallop, J. Org. Chem. 59, 7588-7590 (1994).
21. F. Albericio, M. Pons, E. Pedroso, and E. Giralt, J. Org. Chem. 54, 360-366 (1989).
22. M. Mazure, B. Calas, A. Cavé, and J. Parello, C.R. Acad. Sci. Ser. 2303, 553-556 (1986).
23. A. G. Ludwick, L. W. Jelinski, D. Live, A. Kintanar, and J. J. Dumais, J. Am. Chem. Soc. 108, 6493-6496 (1986).
24. F. Bardella, R. Eritja, E. Pedroso, and E. Giralt, Bioorg. Med. Chem. Lett. 3, 2793-2796 (1993).
25. D. L. Vanderhart, W. L. Earl, and A. N. Garroway, J. Magn. Reson. 44, 361-401 (1981).
26. J. B. Wooten, J. Agric. Food. Chem. 33, 419-425 (1985).
27. C. S. Springer, Jr., in "NMR in Physiology and Biomedicine" (R. J. Gillies, Ed.), Chap. 5, Academic Press, San Diego, 1994.
28. S. C. K. Chu, Y. Xu, J. A. Balschi, and C. S. Springer, Jr., Magn. Reson. Med. 13, 239-262 (1990).
29. P. T. Callaghan, "Principles of Nuclear Magnetic Resonance Microscopy," pp. 208-242, Clarendon Press, Oxford, 1991.
30. M. E. Stoll and T. J. Majors, J. Phys. Rev. 624, 2859-2862 (1981).
31. D. Doskocilová, D. D. Tao, and B. Schneider, Czech. J. Phys. B 25, 202-209 (1975).
32. A. N. Garroway, J. Magn. Reson. 49, 168-171 (1982).
33. D. T. Edmonds and M. R. Wormald, J. Magn. Reson. 77, 223-232 (1988).
34. J. Forbes, J. Bowers, X. Shan, L. Moran, E. Oldfield, and M. A. Moscarello, J. Chem. Soc. Faraday Trans. 1 84, 3821-3849 (1988).
35. V. Rutar, M. Kovac, and G. Lahajnar, J. Magn. Reson. 80, 133-138 (1988).
36. T. M. Eads, R. K. Weiler, and A. G. Gaonkar, J. Colloid Interface Sci. 145, 466-477 (1991).
37. T. M. Barbara, J. Magn. Reson. A 109, 265-269 (1994).
38. A. Manzi, P. V. Salimath, R. C. Spiro, P. A. Keifer, and H. H. Freeze, J. Biol. Chem. 270, 9154-9163 (1995).
39. Wilmad Glass Co., Buena, New Jersey.
40. Varian NMR Instruments, Palo Alto, California.
41. Shigemi Inc., Allison Park, Pennsylvania.
42. L. F. Fuks, F. S. C. Huang, C. M. Carter, W. A. Edelstein, and P. B. Roemer, J. Magn. Reson. 100, 229-242 (1992).
43. Obtained from BACHEM, Torrence, California.
44. S. K. Sarkar, R. S. Girigipati, J. L. Adams, and P. A. Keifer, J. Am. Chem. Soc., in press, (1996).
45. P. A. Keifer, J. Org. Chem., in press, (1996).
46. A. D. Buckingham, T. Schaefer, and W. G. Schneider, J. Chem. Phys. 32, 1227-1233 (1960).
47. M. Periyasamy and W. T. Ford, React. Polym. Ion Exch. Sorbents 3, 351-355 (1985).