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(E)-2,4,6-Trimethyl-N-octylideneaniline were prepared by combining the aldehyde and 2,4,6-trimethylamine (5 mmol each) in toluene (5 mL) at 23 °C, removing the solvent under vacuum, filtering the toluene solution of the residue through activated silica gel (0.2 g), and concentrating to afford the pure imine.
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(E)-2,4,6-Trimethyl-N-octylideneaniline were prepared by combining the aldehyde and 2,4,6-trimethylamine (5 mmol each) in toluene (5 mL) at 23 °C, removing the solvent under vacuum, filtering the toluene solution of the residue through activated silica gel (0.2 g), and concentrating to afford the pure imine.
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65249144146
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SHELXTL-NT version 6.12. Structure Determination Package, Bruker-Nonius AXS. Madison, Wisconsin, USA, 2001
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SHELXTL-NT version 6.12. Structure Determination Package, Bruker-Nonius AXS. Madison, Wisconsin, USA, 2001.
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