A combination of ultrasonic assisted extraction with LC-MS/MS for the determination of organophosphorus pesticides in sludge

Analytica Chimica Acta

Volumn 641, Issue 1-2, 2009, Pages 117-123

  García Valcárcel, Ana Isabel ^a   Tadeo, José Luis ^a  

^a INIA   (Spain)

Author keywords

Liquid chromatography tandem mass spectrometry; Organophosphorus pesticides; Sludge; Ultrasonic assisted extraction

Indexed keywords

CHLORPYRIFOS; DIFFERENT SOLVENTS; ION SUPPRESSIONS; LC-MS/MS; LIMITS OF QUANTIFICATIONS; LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY; MATRIX EFFECTS; MATRIXES; NEGATIVE ION; ORGANOPHOSPHORUS PESTICIDES; REAL SLUDGE SAMPLES; SLUDGE; SLUDGE SAMPLES;

ACETONITRILE; AGRICULTURAL CHEMICALS; BODY FLUIDS; CHROMATOGRAPHIC ANALYSIS; CHROMATOGRAPHY; ELECTROSPRAY IONIZATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION CHROMATOGRAPHY; LIQUIDS; MASS SPECTROMETERS; MASS SPECTROMETRY; METABOLISM; METABOLITES; PESTICIDES; SEWAGE SLUDGE; SPECTRUM ANALYSIS; ULTRASONICS;

SOLVENT EXTRACTION;

2,3 DIHYDRO 1H IMIDAZO[1,2 B]PYRAZOLE; ACETONITRILE; ANION; AZAMETHIPHOS; CHLORPYRIFOS; CHLORPYRIFOS METHYL; DICHLORVOS; DIMPYLATE; METHAMIDOPHOS; ORGANOPHOSPHATE PESTICIDE; PIRIMIPHOS METHYL; UNCLASSIFIED DRUG;

ARTICLE; CONTROLLED STUDY; ELECTROSPRAY; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; PURIFICATION; SLUDGE; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY; ULTRASOUND; VALIDATION STUDY;

EID: 64749101416     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2009.03.046     Document Type: Article

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