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Volumn 48, Issue 4, 2009, Pages 1266-1268

Novel polythreaded coordination polymer: From an armed-polyrotaxane sheet to a 3D polypseudorotaxane array, photo-thermochromic behaviors

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EID: 64349124978     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic8021672     Document Type: Article
Times cited : (134)

References (33)
  • 14
    • 64349105110 scopus 로고    scopus 로고
    • Carlucci, L.; Ciani, G.; Proserpio, D. M. Cryst. Growth Des. 2005, 5, 37. (c) Kasai, K.: Sato, M. Chem. Asian J. 2006, 344.
    • (b) Carlucci, L.; Ciani, G.; Proserpio, D. M. Cryst. Growth Des. 2005, 5, 37. (c) Kasai, K.: Sato, M. Chem. Asian J. 2006, 344.
  • 20
    • 64349083563 scopus 로고    scopus 로고
    • H2BpybcCL2 was synthesized by the reported procedure. A solution of CdCl2 2.5H2O (0.05 mmol in 2.0 mL of water) was carefully layered on a mixed solution (the pH value is 7, which is adjusted by a 1 mol L-1 NaOH aqueous solution) of H 2BpybcCl2 (24.8 mg, 0.05 mmol) and FLBDC (8.3 mg, 0.05 mmol) in H,0/DMSO (1.6 mL/0.4 mL) with H2b/DMSO (1.8 mL/0.20 mL) placed between the two layers. Yellow prism crystals of 1 began to form in a few days. Yield: >45, Elem anal. Calcd for C47Cd1H 54N3O20 1093.36, C. 51.67; H, 4.98; N, 3.84. Found: C. 51.98; H, 4.67; N, 3.79
    • 20 (1093.36): C. 51.67; H, 4.98; N, 3.84. Found: C. 51.98; H, 4.67; N, 3.79.
  • 21
    • 64349090200 scopus 로고    scopus 로고
    • Ctystal data for 1: C47Cd1H54N 3O20, Mr, 1093.36, monoclinic, P21/ c, a, 11.986(4) Å, b, 16.002(5) Å. c, 25.926(8) Å, β, 93.814(5)°, V= 4962(3) Å3, T= 294 K, Z= 4, D c, 1.463 g cm-3, μ, 0.520 mm-1, F(000, 2180, GOF, 1.043, a total of 37 482 reflections were collected, 11 126 of which were unique (Rint, 0.0379, Rl, 0.0844, wR2, 0.2529 [I > 2o{horn}I, CCDC 708220
    • int = 0.0379). Rl = 0.0844, wR2 = 0.2529 [I > 2o{horn}(I)]. CCDC 708220.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.