The first two-dimensional polycatenane: A new type of robust network obtained by Ag-connected one-dimensional polycatenanes

Crystal Growth and Design

Volumn 6, Issue 7, 2006, Pages 1566-1568

  Sagué, Jorge L ^a   Fromm, Katharina M ^a  

^a UNIVERSITY OF BASEL   (Switzerland)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 33746728920     PISSN: 15287483     EISSN: None     Source Type: Journal    
DOI: 10.1021/cg060255+     Document Type: Article

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44. -1, F(000) = 644,4984 reflections of which 4984 unique and 4984 observed, 325 parameters refined, GOF = 0.931, R1 = 0.0602, wR2 = 0.1342 for I > 2σ(I) and R1 = 0.1157, wR2 = 0.1584 for all data.
45. -1, F(000) = 3584, 56 024 reflections of which 21 906 unique and 4391 observed, 488 parameters refined, GOF = 1.032, R1 = 0.0698, wR2 = 0.1840 for I > 2σ(I) and R1 = 0.0971, wR2 = 0.2075 for all data.
46. 2 with the SHELX-97 package. All heavy atoms were refined anisotropically. The positions of the hydrogen atoms could be calculated using riding models for all carbon atoms. Crystallographic data for the structures reported here have been deposited with the Cambridge Crystallographic Data Centre as supplementary publications no. CCDC-295448 (1) and CCDC-295449 (2). Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB21EZ, UK (fax: (+44)1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).