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3 solution (10 mL) was then added. The mixture was extracted with EtOAc (2 × 50 mL). The combined organic layers were washed with water (10 mL) and brine (10 mL) and dried over anhydrous sodium sulfate. The solvent was removed and the crude residue purified by silica gel chromatography (PE/EtO Ac).
-
3 solution (10 mL) was then added. The mixture was extracted with EtOAc (2 × 50 mL). The combined organic layers were washed with water (10 mL) and brine (10 mL) and dried over anhydrous sodium sulfate. The solvent was removed and the crude residue purified by silica gel chromatography (PE/EtO Ac).
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