Orthogonal array optimization of microwave-assisted derivatization for determination of trace amphetamine and methamphetamine using negative chemical ionization gas chromatography-mass spectrometry

Journal of Chromatography A

Volumn 1216, Issue 18, 2009, Pages 4083-4089

  Chung, Li Wen ^a   Lin, Keh Liang ^b   Yang, Thomas Ching Cherng ^c   Lee, Maw Rong ^a  

^a NATIONAL CHUNG HSING UNIVERSITY   (Taiwan)

^b CHUNG SHAN MEDICAL UNIVERSITY   (Taiwan)

^c NATIONAL KAOHSIUNG NORMAL UNIVERSITY   (Taiwan)

Author keywords

Analysis of variance; Gas chromatography mass spectrometry; Microwave assisted derivatization; Negative chemical ionization; Orthogonal array design

Indexed keywords

CALIBRATION CURVES; CORRELATION COEFFICIENTS; DERIVATIZATION REAGENTS; EXPERIMENTAL FACTORS; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; IRRADIATION TIME; LIMIT OF DETECTIONS; MICROWAVE POWER; MICROWAVE-ASSISTED DERIVATIZATION; NEGATIVE CHEMICAL IONIZATION; OPTIMUM CONDITIONS; ORTHOGONAL ARRAY DESIGN; ORTHOGONAL ARRAYS; URINE SAMPLES;

AMINES; AMPLITUDE MODULATION; CHEMICAL REACTIONS; CHLORINE COMPOUNDS; CHROMATOGRAPHIC ANALYSIS; GAS CHROMATOGRAPHY; GASES; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IONIZATION OF GASES; IRRADIATION; MASS SPECTROMETERS; MASS SPECTROMETRY; MICROWAVE GENERATION; MICROWAVE IRRADIATION; MICROWAVE POWER TRANSMISSION; REGRESSION ANALYSIS; SOLVENTS; SPECTRUM ANALYSIS; TRACE ANALYSIS;

ANALYSIS OF VARIANCE (ANOVA);

2,3,4,5,6 PENTAFLUOROBENZOYL CHLORIDE; AMPHETAMINE; CHLORIDE; FLUORINE DERIVATIVE; METHAMPHETAMINE; UNCLASSIFIED DRUG;

ANALYTIC METHOD; ARTICLE; CALIBRATION; DERIVATIZATION; IONIZATION; MASS FRAGMENTOGRAPHY; MICROWAVE IRRADIATION; NEGATIVE CHEMICAL IONIZATION GAS CHROMATOGRAPHY MASS SPECTROMETRY; PRIORITY JOURNAL; URINALYSIS;

AMPHETAMINE; BENZOATES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; METHAMPHETAMINE; MICROWAVES; SENSITIVITY AND SPECIFICITY;

EID: 63449108893     PISSN: 00219673     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.chroma.2009.03.020     Document Type: Article

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