Gas chromatography-isotope dilution mass spectrometry preceded by liquid-liquid extraction and chemical derivatization for the determination of ketamine and norketamine in urine

Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences

Volumn 799, Issue 1, 2004, Pages 37-50

  Chou, Su Lien ^a,b   Yang, Mo Hsiung ^a   Ling, Yong Chien ^a   Giang, Yun Seng ^b  

^a NATIONAL TSING HUA UNIVERSITY   (Taiwan)

^b CENTRAL POLICE UNIVERSITY   (Taiwan)

Author keywords

Derivatization, GC; Ketamine; Norketamine

Indexed keywords

AMINES; BODY FLUIDS; CALIBRATION; DRUG PRODUCTS; EXTRACTION; GAS CHROMATOGRAPHY; IONIZATION; MASS SPECTROMETRY; METABOLITES;

DRUG TESTING; LIQUID-LIQUID EXTRACTION (LLE);

BIOMEDICAL ENGINEERING;

BENZOIC ACID DERIVATIVE; DRUG METABOLITE; KETAMINE; NORKETAMINE; PENTAFLUOROBENZOYL CHLORIDE; UNCLASSIFIED DRUG;

ACCURACY; ARTICLE; CALCULATION; CALIBRATION; CORRELATION ANALYSIS; DRUG DETERMINATION; DRUG IDENTIFICATION; GAS CHROMATOGRAPHY; IONIZATION; ISOTOPE DILUTION ASSAY; LIQUID LIQUID EXTRACTION; MASS SPECTROMETRY; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; URINALYSIS;

EID: 0345059172     PISSN: 15700232     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jchromb.2003.10.009     Document Type: Article

References (40)

1. Corssen G., Miyasaka M., Domino E.F. Anesth. Analg. 47(6):1966;746.
2. Kreuscher H., Gauch H. Anesthesia. 16(8):1967;229.
3. Bree M.M., Feller I., Corssen G. Anesth. Analg. 46(5):1967;596.
4. Bree M.M., Gross N.B. Lab. Anim. Care. 19(4):1969;5002.
5. Beck C.C., Coppock R.W., Ott B.S. Vet. Med. Small Anim. Clin. 66(10):1971;993.
6. Curran H.V., Monaghan L. Addiction. 96(5):2001;749.
7. Moore K.A., Kilbane E.M., Jones R., Kunsman G.W., Levine B., Smith M. J. Forensic Sci. 42:1997;1183.
8. Peyton S.C., Couch A.T., Bost R.O. J. Anal. Toxicol. 12:1988;268.
9. Licata M., Pierini P., Popoli G. J. Forensic Sci. 39:1994;1314.
10. DEA Press Release, DEA to control "special K" for the first time, 13 July 1999.
11. Erowid, The vaults of Erowid, http://www.erowid.org/chemicals/ketamine/ ketamine_testing.shtml , 10 Jan 2003.
12. Idvall J., Ahlgren I., Aronsen K.R., Stenberg P. Brit. J. Anaesth. 51:1979;1167.
13. Malinovsky J.M., Servin F., Cozian A., Lepage J.Y., Pinaud M. Brit. J. Anaesth. 77(2):1996;203.
14. Wieber J., Gugler R., Hengstmann J.H., Dengler H.J. Anesthesia. 24:1975;260.
15. Moore K.A., Sklerov J., Levine B., Jacobs A.J. J. Anal. Toxicol. 25(7):2001;583.
16. Adams J.D., Baillie T.A., Trevor A.J., Castagnoli N. Biomed. Mass Spectrosc. 8(11):1981;527.
17. Kochhar M.M. Clin. Toxicol. 11(2):1977;265.
18. Davisson J.N. J. Chromatogr. 146:1978;344.
19. Pitts F.N., Yago L.S., Aniline O. J. Chromatogr. 193:1980;157.
20. Stiller R.I., Dayton P.G., Perel J.M., Hug C.C. J. Chromatogr. 232:1982;305.
21. Olmos-Carmona M.L., Hernandez-Carrasquilla M. J. Chromatogr. B. 734:1999;113.
22. Gross A.S., Nicolay A., Eschalier A. J. Chromatogr. B. 728:1999;107.
23. Gaillard Y., Pepin G. J. Forensic Sci. 43(2):1998;435.
24. Svensson J.-O., Gustafsson L.L. J. Chromatogr. B. 678:1996;373.
25. Sporkert F., Pragst F. Forensic Sci. Int. 107(1):2000;129.
26. Sams R., Pizzo P. J. Anal. Toxicol. 11(2):1987;58.
27. Kochhar M.M., Bavda L.T., Bhushan R.S. Res. Comm. Chem. Pathol. Pharmacol. 14(2):1976;367.
28. S. Cohen (Ed.), Toxi-News [ http://www.erowid.org ] 21 (1) (2002).
29. Olmos-Carmona M.L., Hernandez-Carrasquilla M. J. Chromatogr. B. 734:1999;113.
30. Hodshon B.J., Ferrer-Allado T., Brechner V.L., Cho A.K. Anesthesiology. 36(5):1972;506.
31. Chang T., Glazko A.J. Anesthesiology. 36:1972;401.
32. Williams M.L., Wainer I.W. Therap. Drug Monit. 24:2002;290.
33. Cohen M.L., Trevor A.J. J. Pharmacol. Exp. Therap. 189(2):1974;351.
34. Yanagihara Y., Ohtani M., Kariya S., Uchino K., Aoyama T., Yamamura Y., Iga T. J. Chromatogr. B. 746:2000;227.
35. Bolze S., Boulieu R. Clin. Chem. 44(3):1998;5600.
36. Kharasch E.D., Labroo R. Anesthesiology. 77:1992;1201.
37. R.H. Liu, Elements and Practice in Forensic Drug Urinalysis, Central Police University Press, Taiwan, ROC, 1994.
38. Wang S.-M., Giang Y.-S., Ling Y.-C. J. Chromatogr. B. 759:2001;17.
39. Goldberger B.A., Huestis M.A., Wilkins D.G. Forensic Sci. Rev. 9(2):1997;59.
40. Analytical Methods Committee, Analyst 112 (1987) 199.