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Volumn 8, Issue 9, 2008, Pages 3135-3136

Crystal water of cadmium acetate-dependent formation of one-dimensional channel structure based on 4,4′-bis(1-imidazolyl)biphenyl

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EID: 61549104466     PISSN: 15287483     EISSN: 15287505     Source Type: Journal    
DOI: 10.1021/cg800038j     Document Type: Article
Times cited : (10)

References (47)
  • 5
    • 4444275259 scopus 로고    scopus 로고
    • Kitagawa, S.; Kitaura, R.; Noro, S. Angew. Chem., Int. Ed. 2004, 43, 2334-2375.
    • (e) Kitagawa, S.; Kitaura, R.; Noro, S. Angew. Chem., Int. Ed. 2004, 43, 2334-2375.
  • 39
    • 61549085189 scopus 로고    scopus 로고
    • Recently, Hanson et al. used ligand 3 as a linker to build extended cationic zinc phosphate cluster frameworks. See ref 6b
    • Recently, Hanson et al. used ligand 3 as a linker to build extended cationic zinc phosphate cluster frameworks. See ref 6b.
  • 40
    • 61549094541 scopus 로고    scopus 로고
    • Crystal data for 4: C44H40Cd 2N8O8, M, 1033.64, colorless needle, triclinic, space group P1̄ (No. 2, a, 10.104(3) Å, b, 10.676(4) Å, c, 11.869(4) Å, α, 111.14(3)°, β, 98.22(3)°, γ, 110.32(2)°, V, 1065.9(6) Å3, Z, 1, T, 293(2) K, Dc, 1.610 g/cm3, F(000, 520, reflections collected, 3964, independent reflections, 3913 Rint, 0.0111, Å, 0.0492, wR2, 0.1139, GOF, 0.986
    • 2 = 0.1139, GOF = 0.986.
  • 41
    • 61549107435 scopus 로고    scopus 로고
    • The purities of bulk samples of crystals 4 and 6 were determined through comparison of experimental and simulated PXRD patterns. Their experimental patterns favorably correlate with the corresponding simulated ones generated from single-crystal X-ray diffraction data. Unfortunately, crystal 5 immediately collapsed after being removed from the mother liquor, and reliable powder X-ray as well as elemental analysis data could not be obtained thereby. See Figures S1 and S2 in the Supporting Information, 11) The exact number of guest molecules (solvents) in the crystallographic asymmetry unit can not be determined according to the Fourier electron-densities because of disorder. However, the host framework can be located exactly. Crystal data for 5: Colorless plates, triclinic, space group P1̄ (No. 2, a, 5.6528(11) Å, b, 9.887(3) Å, c, 12.924(3) Å, Å, 75.29(2)°, β, 80.906(19)°, γ, 77.244(19)°, V, 677.43
    • 2 = 0.1658, GOF = 0.993.
  • 43
    • 61549103331 scopus 로고    scopus 로고
    • Crystal data for 6: C22H22CdN 4O5, M, 534.84, colorless needle, triclinic, space group P1̄ (No. 2, a, 9.260(3) Å, b, 10.595(3) Å, c, 11.532(3) Å, α, 90.07(2)°, β, 102.86(2)°, γ, 103.33(2)°, V, 1071.7(5) Å3, Z, 2, T, 293(2) K, Dc, 1.657 g/cm3, F(000, 540, reflections collected, 3968, independent reflections, 3827 Rint, 0.0043, R1, 0.0487, wR2, 0.1166, GOF, 1.034
    • 2 = 0.1166, GOF = 1.034.
  • 44
    • 33749652262 scopus 로고    scopus 로고
    • Selected examples of water-filled channels in metal organic framework structures: (a) Hu, L.; Fan, J.; Slebodnick, C.; Hanson, B. E. Inorg. Chem. 2006, 45, 7681-7688.
    • Selected examples of water-filled channels in metal organic framework structures: (a) Hu, L.; Fan, J.; Slebodnick, C.; Hanson, B. E. Inorg. Chem. 2006, 45, 7681-7688.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.