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Crystallographic data for 2: C32H46B 2N4Si4, M, 620.71, a, 6.8710(7) Å, b, 19.769(2) Å, c, 12.6216(13) Å, b, 99.396(2)°, V, 1691.4(3) Å3, Z, 2, space group P21/c, T, 100(2) K, λ, 0.710 73 Å, Dcalcd, 1.219 Mg·m-3, m, 0.204 mm-1, R(F, Fo > 4σ(Fo, 0.0443, wRF2, all unique data, 0.1333
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60849099877
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Crystallographic data for 5: C42H66Al 2N4O2Si4, M, 825.31, a, 7.1890(18) Å, b, 16.902(4) Å, c, 19.026(5) Å, b, 99.223(5)°, V, 2282(1) Å3, Z, 2, space group P21/n, T, 100(2) K, λ, 0.710 73 Å, Dcalcd, 1.201 Mg·m-3, m, 0.207 mm-1, R(F, F o > 4σ(Fo, 0.0508, wRF 2, all unique data, 0.1341
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2) [all unique data] = 0.1341.
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