Imino-indolate half-titanocene chlorides: Synthesis and their ethylene (Co-)polymerization

Journal of Polymer Science, Part A: Polymer Chemistry

Volumn 47, Issue 2, 2009, Pages 357-372

  Zuo, Weiwei ^a   Zhang, Min ^a   Sun, Wen Hua ^a  

^a INSTITUTE OF CHEMISTRY   (China)

Author keywords

Copolymerization; Metallocene catalysts; Organometallic catalysts; Polyethylene

Indexed keywords

CATALYSIS; CATALYST ACTIVITY; CATALYSTS; CHELATION; CHEMICAL REACTIONS; CHLORINE COMPOUNDS; COBALT; ELECTROCHEMICAL SENSORS; ETHYLENE; LIGANDS; MOLECULAR WEIGHT; MONOMERS; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; ORGANOMETALLICS; POLYMERIZATION; POLYMERS; POLYOLEFINS; SINGLE CRYSTALS; SODIUM; SYNTHESIS (CHEMICAL); THERMOPLASTICS; TITANIUM COMPOUNDS; X RAY DIFFRACTION ANALYSIS;

ALKYL SUBSTITUENTS; CATALYTIC ACTIVITIES; CATALYTIC SYSTEMS; CYCLOPENTADIENYL; ELEMENTAL ANALYSES; ETHYLENE POLYMERIZATIONS; FUNCTIONALIZED POLYOLEFINS; GPC ANALYSIS; METALLOCENE CATALYSTS; METHYL SUBSTITUENTS; METHYLALUMINOXANE; NMR SPECTROSCOPIES; ORGANOMETALLIC CATALYSTS; TITANOCENE CHLORIDES; TITANOCENES;

COPOLYMERIZATION;

EID: 58349102312     PISSN: 0887624X     EISSN: 10990518     Source Type: Journal    
DOI: 10.1002/pola.23139     Document Type: Article

References (84)

1. Long, W. P.; Breslow, D. S. J Am Chem Soc 1960, 82, 1953-1957.
2. (a) Sinn, H.; Kaminsky, W. Adv Organomet Chem 1980, 18, 99-125;
3. (b) Sinn, H.; Kaminsky, W.; Vollmer, H. J. Angew Chem Int Ed 1980, 19, 390-392.
4. McKnight, A. L.; Waymouth, R. M. Chem Rev 1998, 98, 2587-2598.
5. Aitola, E.; Hakala, K.; Byman-Fagerholm, H.; Leskela, M.; Repo, T. J Polym Sci Part A: Polym Chem 2008, 46, 373-382.
6. Kaminsky, W. J Polym Sci Part A: Polym Chem 2004, 42, 3911-3921.
7. Gibson, V. C.; Spitzmesser, S. K. Chem Rev 2003, 103, 283-316.
8. (a) Herskovics-Korine, D.; Eisen, M. S. J Organomet Chem 1995, 503, 307-314;
9. (b) Flores, J. C.; Chien, J. C. W.; Rausch, M. D. Organometallics 1995, 14, 2106-2108;
10. (c) Volkis, V.; Shmulinson, M.; Averbuj, C.; Lisovskii, A.; Edel-mann, F. T.; Eisen, M. S. Organometallics 1998, 17, 3155-3157.
11. (a) Clark, H. C. S.; Cloke, F. G. N.; Hitchcock, P. B.; Love, J. B.; Wainwright, A. P. J Organomet Chem 1995, 501, 333-340;
12. (b) Scollard, J. D.; McConville, D. H. J Am Chem Soc 1996, 118, 10008-10009;
13. (c) Scollard, J. D.; McConville, D. H.; Payne, N. C.; Vittal, J. J. Marcomolecules 1996, 29, 5241-5243;
14. (d) Horton, A. D.; de With, J.; van der Linden, A. J.; van de Weg, H. Organometallics 1996, 15, 2672-2674;
15. (e) Warren, T. H.; Schrock, R. R.; Davis, W. M. Organometallics 1998, 17, 308-321;
16. (f) Baumann, R.; Davis, W. M.; Schrock, R. R. J Am Chem Soc 1997, 119, 3830-3831;
17. (g) Gibson, V. C.; Kimberley, B. S.; White, A. J. P.; Williams, D. J.; Howard, P. Chem Commun 1998, 3, 313-314.
18. (a) van der Linden, A.; Schaverien, C. J.; Meijboom, N.; Ganter, C.; Orpen, A. G. J Am Chem Soc 1995, 117, 3008-3021;
19. (b) Fokken, S.; Spaniol, T. P.; Kang, H.-C.; Massa, W.; Okuda, J. Organometallics 1996, 15, 5069-5072.
20. (a) Matsui, S.; Tohi, Y.; Mitani, M.; Saito, J.; Makio, H.; Tanaka, H.; Nitabaru, M.; Nakano, T.; Fujita, T. Chem Lett 1999, 10, 1065-1066;
21. (b) Matsui, S.; Mitani, M.; Saito, J.; Tohi, Y.; Makio, H.; Matsukawa, N.; Takagi, Y.; Tsuru, K.; Nitabaru, M.; Nakano, T.; Tanaka, H.; Kashiwa, N.; Fujita, T. J Am Chem Soc 2001, 123, 6847-6856;
22. (c) Makio, H.; Kashiwa, N.; Fujita, T. Adv Synth Catal 2002, 344, 477-493.
23. (a) Yoshida, Y.; Matsui, S.; Takagi, Y.; Mitani, M.; Nakano, T.; Tanaka, H.; Kashiwa, N.; Fujita, T. Organometallics 2001, 20, 4793-4799;
24. (b) Yoshida, Y.; Mohri, J.-I.; Ishii, S.-I.; Mitani, M.; Saito, J.; Matsui, S.; Makio, H.; Nakano, T.; Tanaka, H.; Onda, M.; Yamamoto, Y.; Mizuno, A.; Fujita, T. J Am Chem Soc 2004, 126, 12023-12032;
25. (c) Yoshida, Y.; Matsui, S.; Fujita, T. J Organomet Chem 2005, 690, 4382-4397.
26. (a) Nomura, K.; Liu, J.; Padmanabhan, S.; Kitiyanan, B. J Mol Catal A 2007, 267, 1-29 and references therein;
27. (b) Nomura, K.; Yamada, J.; Wang, W.; Liu, J. J Organomet Chem 2007, 692, 4675-4682;
28. (c) Itagaki, K.; Fujiki, M.; Nomura, K. Marcomolecules 2007, 40, 6489-6499;
29. (d) Zhang, H.; Byun, D. J.; Nomura, K. Dalton Trans 2007, 18, 1802-1806;
30. (e) Huang, J.; Lian, B.; Qian, Y.; Zhou, W.; Chen, W.; Zheng, G. Marcomolecules 2002, 35, 4871-4874;
31. (f) Zhang, J.; Lin, Y.-J.; Jin, G.-X. Organometallics 2007, 26, 4042-4047;
32. (g) Stelzig, S. H.; Tamm, M.; Waymouth, R. M. J Polym Sci Part A: Polym Chem 2008, 46, 6064-6070.
33. Zuo, W.; Sun, W.-H.; Zhang, S.; Hao, P.; Shiga, A. J Polym Sci Part A: Polym Chem 2007, 45, 3415-3430.
34. Liu, S.; Zuo, W.; Zhang, S.; Hao, P.; Li, P.; Wang, D.; Sun, W.-H. J Polym Sci Part A: Polym Chem 2008, 46, 3411-3423.
35. Zuo, W.; Zhang, S.; Liu, S.; Liu, X.; Sun, W.-H. J Polym Sci Part A: Polym Chem 2008, 46, 3396-3410.
36. Li, J.; Gao, T.; Zhang, W.; Sun, W.-H. Inorg Chem Commun 2003, 6, 1372-1374.
37. Sheldrick, G. M., SHELXTL-97, Program for the Refinement of Crystal Structures, University of Gottingen, Germany, 1997.
38. (a) Chen, Q.; Huang, J.; Yu, J. Inorg Chem Commun 2005, 8, 444-448;
39. (b) Bott, R. K. J.; Hughes, D. L.; Schormann, M.; Bochmann, M.; Lancaster, S. J. J Organomet Chem 2003, 665, 135-149;
40. (c) Bott, R. K. J.; Schormann, M.; Hughes, D. L.; Lancaster, S. J.; Bochmann, M. Polyhedron 2006, 25, 387-396;
41. (d) Zhang, H.; Katao, S.; Nomura, K.; Huang, J. Organometallics 2007, 26, 5967-5977.
42. (a) Sita, L. R.; Babcock, J. R.; Organometallics 1998, 17, 5228-5230;
43. (b) Doherty, S.; Errington, R. J.; Jarvis, A. P.; Collins, S.; Clegg, W.; Elsegood, M. R. J. Organometallics 1998, 17, 3408-3410.
44. (a) Woo, T. K.; Margl, P. M.; Lohrenz, J. C. W.; Blöhl, P. E.; Ziegler, T. J Am Chem Soc 1996, 118, 13021-13030;
45. (b) Woo, T. K.; Margl, P. M.; Ziegler, T.; Blöhl, P. E. Organometallics 1997, 16, 3454-3468.
46. Sinnema, P.-J.; Hessen, B.; Teuben, J. H. Macromol Rapid Commun 2000, 21, 562-566.
47. (a) Hong, H.; Zhang, Z.; Chung, T. C.; Lee, R. W. J Polym Sci Part A: Polym Chem 2007, 45, 639-649;
48. (b) Smit, M.; Zheng, X.; Loos, J.; Chadwick, J. C;. Koning, C. E. J Polym Sci Part A: Polym Chem 2006, 44, 6652-6657.
49. (a) Yano, A.; Gasegawa, S.; Kaneko, T.; Sone, M.; Sato, M.; Akimoto, A.; Macromol Chem Phys 1999, 200, 1542-1553;
50. (b) Quijiada, R.; Galland, G. B.; Mauler, R. S.; de Menezes, S. C. Macromol Rapid Commun 1996, 17, 607-613;
51. (c) Chu, K.-J.; Soares, J. B. P.; Penlidis, A. Macromol Chem Phys 2000, 201, 340-348;
52. (d) Zhang, Y.; Yang, X.; Yu, Y.; Qian, Y.; Huang, J.; Chin J Chem 2005, 23, 1081-1084;
53. (e) Czaja, K.; Bialek, M. Polymer 2001, 42, 2289-2297.
54. Boffa, L. S.; Novak, B. M. Chem Rev 2000, 100, 1479-1493.
55. (a) Purgett, M. D.; Vogl, O. J Polym Sci Part A: Polym Chem 1989, 27, 2051-2063;
56. (b) Aaltonen, P.; Löfgren, B. Macromolecules 1995, 28, 5353-5357;
57. (c) Hakala, K.; Löfgren, B.; Helaja, T. Eur Polym J 1998, 34, 1093-1097;
58. (d) Schulz, D. N.; Kitano, K.; Burkm, T. J.; Langer, A. W. US Patent 1984; 4, 518, 757;
59. (e) Zhang, X.; Chen, S.; Li, H.; Zhang, Z.; Lu, Y.; Wu, C.; Hu, Y. J Polym Sci Part A: Polym Chem 2007, 45, 59-68.
60. (a) Sun, J.; Shan, Y.; Xu, Y.; Cui, Y.; Schumann, H.; Hummert, M. J Polym Sci Part A: Polym Chem 2004, 42, 6071-6080;
61. (b) Heinemann, J.; Mülhaupt, R.; Brinkmann, P.; Luinstra, G. Macromol Chem Phys 1999, 200, 384-389;
62. (c) Liu, W.; Malinoski, J. M.; Brookhart, M Organometallics 2002, 21, 2836-2838.
63. Huang, Y.; Yang, K.; Dong, J. Macromol Rapid Commun 2006, 27, 1278-1283.
64. (a) Galland, G. B.; de Souza, R. F.; Mauler, R. S.; Nunes, F. F. Macromolecules 1999, 32, 1620-1625;
65. (b) Cheng, H. N. Polym Bull 1986, 16, 445-452;
66. (c) Hansen, E. W.; Blom, R.; Bade, O. M. Polymer 1997, 38, 4295-4304;
67. (d) Hansen, E. W.; Redford, K.; Oysaed, H. Polymer 1996, 37, 19-24.
68. (a) Liu, W.; Rinaldi, P. L.; McIntosh, L. H.; Quirk, R. P. Macromolecules 2001, 34, 4757-4767;
69. (b) Qiu, X.; Redwine, D.; Gobbi, G.; Nuamthanom, A.; Rinaldi, P. L. Macromolecules 2007, 40, 6879-6884.
70. Madorsky, S. L. Thermal Degradation of Organic Polymers; Wiley: New York, 1964.
71. (a) Boor, J. Ziegler-Natta Catalysts and Polymerizations; Academic Press: New York, 1979;
72. (b) Ramakrishnan, S.; Berluche, E.; Chung, T. C. Macromolecules 1990, 23, 378-382.
73. (a) Wendt, R. A.; Fink, G. Macromol Chem Phys 2000, 201, 1365-1373;
74. (b) Hakala, K.; Helaja, T.; Lofgren, B. J Polym Sci Part A: Polym Chem 2000, 38, 1966-1971;
75. (c) Hagihara, H.; Murata, M.; Uozumi, T. Macromol Rapid Commun 2001, 22, 353-357;
76. (d) Imuta, J.; Kashiwa, N.; Toda, Y. J Am Chem Soc 2002, 124, 1176-1177;
77. (e) Hagihara, H.; Tsuchihara, K.; Takeuchi, K.; Murata, M.; Ozaki, H.; Shiono, T. J Polym Sci Part A: Polym Chem 2004, 42, 52-58;
78. (f) Hagihara, H.; Tsuchihara, K.; Sugiyama, J.; Takeuchi, K.; Shiono, T. Macromolecules 2004, 37, 5145-5148;
79. (g) Wendt, R. A.; Angermund, K.; Jensen, V.; Thiel, W.; Fink, G. Macromol Chem Phys 2004, 205, 308-318;
80. (h) Inoue, Y.; Matsugi, T.; Kashiwa, N.; Matyjaszewski, K. Macromolecules 2004, 37, 3651-3658;
81. (I) Hagihara, H.; Ishihara, T.; Theban, H.; Shiono, T. J Polym Sci Part A: Polym Chem 2008, 46, 1738-1748.
82. (a) Kang, K. K.; Shiono, T.; Jeong, Y.-T.; Lee, D.-H. J Macromol Sci Pure Appl Chem 1998, A35, 1003-1016;
83. (b) Aaltonen, P.; Löfgren, B. Eur Polym J 1997, 33, 1187-1190.
84. Purgett, M. D.; Vogl, O. J Polym Sci Part A: Polym Chem 1988, 26, 677-700.