N.m.r. characterization of polyethylene with emphasis on internal consistency of peak intensities and estimation of uncertainties in derived branch distribution numbers

Polymer

Volumn 38, Issue 17, 1997, Pages 4295-4304

  Hansen, Eddy W ^a   Blom, Richard ^a   Bade, Otto M ^a  

^a SINTEF   (Norway)

Author keywords

Chemical shift; Peak assignment; Polyethylene

Indexed keywords

CARBON; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; RELAXATION PROCESSES;

CHEMICAL SHIFT; NUCLEAR OVERHAUSER ENHANCEMENT; PEAK INTENSITY; SPIN LATTICE RELAXATION;

LOW DENSITY POLYETHYLENES;

EID: 0031212952     PISSN: 00323861     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0032-3861(96)01027-0     Document Type: Article

References (21)

1. Randall, J. C., J. Polym. Sci., 1973, 11, 275.
2. Cudby, M. E. A. and Bunn, A., Polymer, 1976, 17, 345.
3. McRae, M. A., Makromol. Chem., 1976, 177, 449.
4. Baker, C. and Maddams, W. F., Makromol. Chem., 1976, 177, 449.
5. Axelson, D. E., Mandelkern, L. and Levy, G. C., Macromolecules, 1977, 10, 557.
6. Axelson, D. E., Levy, G. C. and Mandelkern, L., Macromolecules, 1979, 12, 41.
7. Randall, J. C. and Hsieh, E. T., NMR and Macromolecules, ACS Symposium Series 247, ed. J. C. Randall. Am. Chem. Soc., Washington, DC, 1984, Chap. 9.
8. Freche, P. and Grenier-Loustalot, M.-F., J. Eur. Polym., 1984, 20, 31.
9. Usami, T. and Takayama, S., Macromolecules, 1984, 17, 1756.
10. Cheng, H. N., Polym. Bull., 1986, 16, 445.
11. Bugada, D. C. and Rudin, A., Eur. Polym. J., 1987, 23, 809.
12. Usami, T., Gotoh, Y., Takayama, S., Ohtani, H. and Tsuge, S., Macromolecules, 1987, 20, 1557.
13. Randall, J. C., J. Macromol. Sci.-Rev. Macromol. Chem. Phys. (C), 1989,29, 201.
14. De Pooter, M., Smith, P. B., Dohrer, K. K., Bennett, K. F., Meadows, M. D., Smith, C. G., Schouwenaars, H. P. and Geerards, R. A., J. Appl. Polym. Sci., 1991, 42, 399.
15. Delpuech, J.-J. (ed.), Dynamics of Solutions and Fluid Mixtures by NMR. John Wiley and Sons, England, 1995.
16. Bovey, F. A., Nuclear Magnetic Resonance Spectroscopy, 2nd edn. Academic Press, Inc., London, 1988.
17. Horii, F., Zhu, Q., Kitamoru, R. and Yamaoka, H., Macromolecules, 1990, 23, 977.
18. Bade, O. M. and Blom, R., J. Appl. Cat., 1997, in press..
19. Lindemann, L. P. and Adams, J. Q., Anal. Chem., 1971, 43, 1245.
20. Harris, R. K., Nuclear Magnetic Resonance Spectroscopy, a Physical View. Pitman Books Limited, London, 1983.
21. Hay, J. N., Mills, P. J. and Ognjanovic, R., Polymer, 1986, 27, 677.