Quantification of monomer elution and carbon-carbon double bonds in dental adhesive systems using HPLC and micro-Raman spectroscopy

Journal of Dentistry

Volumn 37, Issue 3, 2009, Pages 177-184

  Miletic, Vesna ^a   Santini, Ario ^a   Trkulja, Ivan ^a  

^a UNIVERSITY OF EDINBURGH   (United Kingdom)

Author keywords

Adhesive; Degree of conversion; Dimethacrylate; Elution; HPLC; Monomer; Ormocer; Raman; Silorane

Indexed keywords

DENTIN BONDING AGENT; METHACRYLIC ACID DERIVATIVE; RESIN CEMENT;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; DENTAL ACID ETCHING; DENTAL BONDING; DENTIN; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; METHODOLOGY; PHASE TRANSITION; RAMAN SPECTROMETRY;

ACID ETCHING, DENTAL; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DENTAL BONDING, LIGHT-CURED; DENTIN; DENTIN-BONDING AGENTS; HUMANS; METHACRYLATES; MOLECULAR STRUCTURE; PHASE TRANSITION; RESIN CEMENTS; SPECTRUM ANALYSIS, RAMAN;

EID: 58249129300     PISSN: 03005712     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jdent.2008.11.006     Document Type: Article

References (39)

1. Bae J.H., Cho B.H., Kim J.S., Kim M.S., Lee I.B., Son H.H., et al. Adhesive layer properties as a determinant of dentin bond strength. Journal of Biomedical Material Research Part B: Applied Biomaterials 74 (2005) 822-828
2. Cadenaro M., Antoniolli F., Sauro S., Tay F.R., Di Lenarda R., Prati C., et al. Degree of conversion and permeability of dental adhesives. European Journal of Oral Sciences 113 (2005) 525-530
3. Nunes T.G., Garcia F.C., Osorio R., Carvalho R., and Toledano M. Polymerization efficacy of simplified adhesive systems studied by NMR and MRI techniques. Dental Materials 22 (2006) 963-972
4. Emami N., and Soderholm K.J. How light irradiance and curing time affect monomer conversion in light-cured resin composites. European Journal of Oral Sciences 111 (2003) 536-542
5. Witzel M.F., Calheiros F.C., Goncalves F., Kawano Y., and Braga R.R. Influence of photoactivation method on conversion, mechanical properties, degradation in ethanol and contraction stress of resin-based materials. Journal of Dentistry 33 (2005) 773-779
6. Yap A.U., Soh M.S., Han T.T., and Siow K.S. Influence of curing lights and modes on cross-link density of dental composites. Operative Dentistry 29 (2004) 410-415
7. Sasaki N., Okuda K., Kato T., Kakishima H., Okuma H., Abe K., et al. Salivary bisphenol-A levels detected by ELISA after restoration with composite resin. Journal of Material Science: Materials in Medicine 16 (2005) 297-300
8. Geurtsen W., Lehmann F., Spahl W., and Leyhausen G. Cytotoxicity of 35 dental resin composite monomers/additives in permanent 3T3 and three human primary fibroblast cultures. Journal of Biomedical Material Research 41 (1998) 474-480
9. Geurtsen W., Spahl W., Muller K., and Leyhausen G. Aqueous extracts from dentin adhesives contain cytotoxic chemicals. Journal of Biomedical Material Research 48 (1999) 772-777
10. Lewis J.B., Rueggeberg F.A., Lapp C.A., Ergle J.W., and Schuster G.S. Identification and characterization of estrogen-like components in commercial resin-based dental restorative materials. Clinical Oral Investigations 3 (1999) 107-113
11. Nomura Y., Ishibashi H., Miyahara M., Shinohara R., Shiraishi F., and Arizono K. Effects of dental resin metabolites on estrogenic activity in vitro. Journal of Material Science: Materials in Medicine 14 (2003) 307-310
12. Ferracane J.L. Elution of leachable components from composites. Journal of Oral Rehabilitation 21 (1994) 441-452
13. Ferracane J.L., and Condon J.R. Rate of elution of leachable components from composite. Dental Materials 6 (1990) 282-287
14. Michelsen V.B., Lygre H., Skalevik R., Tveit A.B., and Solheim E. Identification of organic eluates from four polymer-based dental filling materials. European Journal of Oral Sciences 111 (2003) 263-271
15. Uzunova Y., Lukanov L., Filipov I., and Vladimirov S. High-performance liquid chromatographic determination of unreacted monomers and other residues contained in dental composites. Journal of Biochemical & Biophysical Methods 70 (2008) 883-888
16. Yap A.U., Han V.T., Soh M.S., and Siow K.S. Elution of leachable components from composites after LED and halogen light irradiation. Operative Dentistry 29 (2004) 448-453
17. Kim J.G., and Chung C.M. Elution from light-cured dental composites: comparison of trimethacrylate and dimethacrylate as base monomers. Journal of Biomedical Material Research Part B: Applied Biomaterials 72 (2005) 328-333
18. Munksgaard E.C., Peutzfeldt A., and Asmussen E. Elution of TEGDMA and BisGMA from a resin and a resin composite cured with halogen or plasma light. European Journal of Oral Sciences 108 (2000) 341-345
19. Sideridou I.D., and Achilias D.S. Elution study of unreacted Bis-GMA, TEGDMA, UDMA, and Bis-EMA from light-cured dental resins and resin composites using HPLC. Journal of Biomedical Material Research Part B: Applied Biomaterials 74 (2005) 617-626
20. Zhang Y., and Xu J. Effect of immersion in various media on the sorption, solubility, elution of unreacted monomers, and flexural properties of two model dental composite compositions. Journal of Material Science: Materials in Medicine 19 (2008) 2477-2483
21. Eliades T., Eliades G., Brantley W.A., and Johnston W.M. Residual monomer leaching from chemically cured and visible light-cured orthodontic adhesives. American Journal of Orthodontics & Dentofacial Orthopedics 108 (1995) 316-321
22. Eliades T., Hiskia A., Eliades G., and Athanasiou A.E. Assessment of bisphenol-A release from orthodontic adhesives. American Journal of Orthodontics & Dentofacial Orthopedics 131 (2007) 72-75
23. Salz U., Zimmermann J., Zeuner F., and Moszner N. Hydrolytic stability of self-etching adhesive systems. Journal of Adhesive Dentistry 7 (2005) 107-116
24. Silikas N., and Watts D.C. High pressure liquid chromatography of dentin primers and bonding agents. Dental Materials 16 (2000) 81-88
25. Kaga M., Noda M., Ferracane J.L., Nakamura W., Oguchi H., and Sano H. The in vitro cytotoxicity of eluates from dentin bonding resins and their effect on tyrosine phosphorylation of L929 cells. Dental Materials 17 (2001) 333-339
26. Van Landuyt K.L., Snauwaert J., De Munck J., Peumans M., Yoshida Y., Poitevin A., et al. Systematic review of the chemical composition of contemporary dental adhesives. Biomaterials 28 (2007) 3757-3785
27. Moon H.-J., Lim B.-S., Lee Y.-K., and Kim C.-W. Determination of residual monomers in dental pit and fissure sealants using food/oral simulating fluids. Bulletin of the Korean Chemical Society 21 (2000) 1115-1118
28. Tay F.R., and Pashley D.H. Aggressiveness of contemporary self-etching systems. I. Depth of penetration beyond dentin smear layers. Dental Materials 17 (2001) 296-308
29. Wang J.D., and Hume W.R. Diffusion of hydrogen ion and hydroxyl ion from various sources through dentine. International Endodontic Journal 21 (1988) 17-26
30. Hashimoto M., Ito S., Tay F.R., Svizero N.R., Sano H., Kaga M., et al. Fluid movement across the resin-dentin interface during and after bonding. Journal of Dental Research 83 (2004) 843-848
31. Santini A., and Miletic V. Comparison of the hybrid layer formed by Silorane adhesive, one-step self-etch and etch and rinse systems using confocal micro-Raman spectroscopy and SEM. Journal of Dentistry 36 (2008) 683-691
32. 13C NMR and simulation using a kinetic gelation model. Macromolecules 22 (1989) 3555-3561
33. Olea N., Pulgar R., Perez P., Olea-Serrano F., Rivas A., Novillo-Fertrell A., et al. Estrogenicity of resin-based composites and sealants used in dentistry. Environmental Health Perspectives 104 (1996) 298-305
34. Hanks C.T., Strawn S.E., Wataha J.C., and Craig R.G. Cytotoxic effects of resin components on cultured mammalian fibroblasts. Journal of Dental Research 70 (1991) 1450-1455
35. Kostoryz E.L., Tong P.Y., Strautman A.F., Glaros A.G., Eick J.D., and Yourtee D.M. Effects of dental resins on TNF-alpha-induced ICAM-1 expression in endothelial cells. Journal of Dental Research 80 (2001) 1789-1792
36. Ratanasathien S., Wataha J.C., Hanks C.T., and Dennison J.B. Cytotoxic interactive effects of dentin bonding components on mouse fibroblasts. Journal of Dental Research 74 (1995) 1602-1606
37. Schweikl H., Spagnuolo G., and Schmalz G. Genetic and cellular toxicology of dental resin monomers. Journal of Dental Research 85 (2006) 870-877
38. Peutzfeldt A. Resin composites in dentistry: the monomer systems. European Journal of Oral Sciences 105 (1997) 97-116
39. Hotta M., Kondoh K., and Kamemizu H. Effect of primers on bonding agent polymerization. Journal of Oral Rehabilitation 25 (1998) 792-799