Ag3Bi14Br21: A subbromide with Bi 24+- dumbbells and Bi95+ polyhedra - Synthesis, crystal structure and chemical bonding;Ag3Bi14Br21: Ein subbromid mit Bi 24+-hanteln und Bi95+-polyedern - Synthese, kristallstruktur und chemische bindung

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 634, Issue 15, 2008, Pages 2873-2879

  Wahl, Bernhard ^a   Ruck, Michael ^a  

^a DRESDEN UNIVERSITY OF TECHNOLOGY   (Germany)

Author keywords

Bismuth; Cluster; Electron localization indicator; Low valent compounds; Silver

Indexed keywords

EID: 57349164277     PISSN: 00442313     EISSN: 15213749     Source Type: Journal    
DOI: 10.1002/zaac.200800320     Document Type: Article

References (85)

1. a) S. Ulvenlund, L. Bengtsson-Kloo, in: Metal Clusters in Chemistry, P. Braunstein, P. R. Raithby, L. A. Oro (eds), Wiley-VCH, Weinheim - New York 1999, p. 561;
2. b) R. B. King, P. von R. Schleyer, G. Linti, H. Schnöckel, W. Uhl, N. Wiberg, P. P. Power, I. Krossing, W. S. Scheldrick, in: Molecular Clus ters of the Main Group Elements, M. Driess, H. Nöth (eds), Wiley-VCH, Weinheim 2004;
3. c) L. Balázs, H. J. Breunig, Coord. Chem. Rev. 2004, 248, 603;
4. d) A. Schnepf, Coord. Chem. Rev. 2006, 250, 2758;
5. e) M. Wendorff, C. Röhr, Z. Anorg. Allg. Chem. 2006, 632, 1792;
6. f) A. Spiekermann, S. D. Hoffmann, T. F. Fässler, I. Krossing, U. Preiss, Angew. Chem. 2007, 119, 5404;
7. Angew. Chem. Int. Ed. 2007, 46, 5310.
8. a) E. Zintl, Angew. Chem. 1939, 52, 1;
9. b) H. Schäfer, B. Eisenmann, W. Müller, Angew. Chem. 1973, 85, 742;
10. Angew. Chem. Int. Ed. Engl. 1973, 12, 694;
11. c) H. G. von Schnering, Angew. Chem. 1981, 93, 44;
12. Angew. Chem. Int. Ed. Engl. 1981, 20, 33;
13. d) R. Nesper, Angew. Chem. 1991, 103, 805;
14. Angew. Chem. Int. Ed. Engl. 1991, 30, 789;
15. e) S. M. Kauzlarich (ed), Chemistry, Structure, and Bonding of Zintl Phases and Ions, VCH Publishers, New York 1996;
16. f) J. D. Corbett, Angew. Chem. 2000, 112, 682;
17. Angew. Chem. Int. Ed. Engl. 2000, 39, 670;
18. g) S. C. Sevov, in: Intermetallic Compounds, Principles and Practice: Progress, J. H. Westbrook, R. L. Freisher (eds), Wiley, Chichester 2002, p. 113;
19. f) A. M. Guloy, R. Ramlau, Z. Tang, W. Schnelle, M. Baitinger, Y. Grin, Nature 2006, 443, 320.
20. M. Ruck, Angew. Chem. 2001, 113, 1222;
21. Angew. Chem. Int. Ed. 2001, 40, 1182.
22. M. Ruck, Solid State Sci. 2001, 3, 369.
23. M. Ruck, R. M. Heich, Z. Anorg. Allg. Chem. 2000, 626, 2449.
24. S. Hampel, M. Ruck, Z. Anorg. Allg. Chem. 2006, 632, 1150.
25. a) K. Wade, Adv. Inorg. Chem. Radiochem. 1976, 18, 1;
26. b) D. M. P. Mingos, Acc. Chem. Res. 1984, 17, 311.
27. a) J. D. Corbett, Inorg. Chem. 1968, 7, 198;
28. b) B. Krebs, M. Mummert, C. Brendel, J. Less-Common Met. 1986, 116, 159;
29. c) S. Ulvenlund, K. Sta;anhl, L. Bengtsson-Kloo, Inorg. Chem. 1996, 35, 223;
30. d) M. Ruck, F. Steden, Z. Anorg. Allg. Chem. 2007, 633, 1556.
31. M. Lindsjö, A. Fischer, L. Kloo, Eur. J. Inorg. Chem. 2005, 670.
32. A. N. Kuznetsov, B. A. Popovkin, K. Sta;anhl, M. Lindsjö, L. Kloo, Eur. J. Inorg. Chem. 2005, 4907.
33. a) M. Ruck, Z. Anorg. Allg. Chem. 1998, 624, 521;
34. b) M. Ruck, S. Hampel, Polyhedron 2002, 21, 651.
35. a) B. Krebs, M. Hucke, C. J. Brendel, Angew. Chem. 1982, 94, 453;
36. Angew. Chem. Int. Ed. Engl. 1982, 21, 445;
37. b) A. N. Kuznetsov, B. A. Popovkin, Z. Anorg. Allg. Chem. 2002, 628, 2179.
38. a) R. M. Friedman, J. D. Corbett, Inorg. Chim. Acta 1973, 7, 525;
39. b) J. Beck, T. Hilbert, Eur. J. Inorg. Chem. 2004, 2019.
40. M. Lindsjö, A. Fischer, L. Kloo, Angew. Chem. 2004, 116, 2594;
41. Angew. Chem. Int. Ed. Engl. 2004, 43, 2540.
42. a) M. Ruck, V. Dubenskyy, T. Söhnel, Angew. Chem. 2003, 115, 3086;
43. Angew. Chem. Int. Ed. 2003, 42, 2978;
44. b) V. Dubenskyy, M. Ruck, Z. Anorg. Allg. Chem. 2004, 630, 2458;
45. c) B. Wahl, V. Dubenskyy, M. Ruck, Z. Kristallogr. Suppl. 2006, 24, 143;
46. d) B. Wahl, L. Kloo, M. Ruck, Angew. Chem. 2008, 120, 3996;
47. Angew. Chem. Int. Ed. 2008, 47, 3932.
48. B. Wahl, M. Ruck, Z. Anorg. Allg. Chem. 2008, 634, 2267.
49. a) A. Hershaft, J. D. Corbett, Inorg. Chem. 1963, 2, 979;
50. b) A. Hershaft, J. D. Corbett, J. Chem. Phys. 1962, 36, 551;
51. c) J. Beck, C. J. Brendel, L. Bengtsson-Kloo, B. Krebs, M. Mummert, A. Stankowski, S. Ulvenlund, Chem. Ber. 1996, 129, 1219;
52. d) M. Ruck, V. Dubenskyy, Z. Anorg. Allg. Chem. 2003, 629, 375;
53. e) A. N. Kuznetsov, P. I. Naumenko, B. A. Popovkin, L. Kloo, Russ. Chem. Bull. 2003, 52, 2100;
54. f) S. Hampel, P. Schmidt, M. Ruck, Z. Anorg. Allg. Chem. 2005, 631, 272.
55. H. von Benda, A. Simon, W. Bauhofer, Z. Anorg. Allg. Chem. 1978, 438, 53.
56. a) R. M. Friedman, J. D. Corbett, Inorg. Chem. 1973, 12, 1134;
57. b) A. N. Kuznetsov, A. V. Shevel'kov, S. I. Troyanov, B. A. Popovkin, Zh. Neorg. Khim. 1996, 41, 958;
58. Russ. J. Inorg. Chem. 1996, 41, 920;
59. c) A. N. Kuznetsov, A. V. Shevel'kov, B. A. Popovkin, Koord. Khim. 1998, 24, 919;
60. Russ. J. Coord. Chem. 1998, 24, 861;
61. A. N. Kuznetsov, L. Kloo, M. Lindsjö, J. Rosdahl, H. Stoll, Chem. Eur. J. 2001, 7, 2821.
62. X-SHAPE, Crystal Optimisation for Numerical Absorption Correction Program, Version 1.06, Stoe & Cie GmbH, Darmstadt 1999.
63. X-RED32, Data Reduction Program, Version 1.01, Stoe & Cie GmbH, Darmstadt 2001.
64. G. M. Sheldrick, Acta Crystallogr. 2008, A64, 112.
65. K. Brandenburg, Diamond 3.1f, Crystal and Molecular Structure Visualization, Crystal Impact GbR, Bonn 2008.
66. M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, J. A. Montgomery, Jr., T. Vreven, K. N. Kudin, J. C. Burant, J. M. Millam, S. S. Iyengar, J. Tomasi, V. Barone, B. Mennucci, M. Cossi, G. Scalmani, N. Rega, G. A. Petersson, H. Nakatsuji, M. Hada, M. Ehara, K. Toyota, R. Fukuda, J. Hasegawa, M. Ishida, T. Nakajima, Y. Honda, O. Kitao, H. Nakai, M. Klene, X. Li, J. E. Knox, H. P. Hratchian, J. B. Cross, C. Adamo, J. Jaramillo, R. Gomperts, R. E. Stratmann, O. Yazyev, A. J. Austin, R. Cammi, C. Pomelli, J. W. Ochterski, P. Y. Ayala, K. Morokuma, G. A. Voth, P. Salvador, J. J. Dannenberg, V. G. Zakrzewski, S. Dapprich, A. D. Daniels, M. C. Strain, O. Farkas, D. K. Malick, A. D. Rabuck, K. Raghavachari, J. B. Foresman, J. V. Ortiz, Q. Cui, A. G. Baboul, S. Clifford, J. Cioslowski, B. B. Stefanov, G. Liu, A. Liashenko, P. Piskorz, I. Komaromi, R. L. Martin, D. J. Fox, T. Keith, M. A. Al-Laham, C. Y. Peng, A. Nanayakkara, M. Challacombe, P. M. W. Gill, B. Johnson, W. Chen, M. W. Wong, C. Gonzalez, and J. A. Pople, Gaussian 03, Revision C.02, Gaussian, Inc., Wallingford CT, 2004.
67. K. A. Peterson, D. Figgen, E. Goll, H. Stoll, M. Dolg, J. Chem. Phys. 2003, 119, 11113.
68. K. A. Peterson, J. Chem. Phys. 2003, 119, 11099.
69. B. Metz, H. Stoll, M. Dolg, J. Chem. Phys. 2000, 113, 2563.
70. a) M. Kohout, Int. J. Quantum Chem. 2004, 97, 651;
71. b) M. Kohout, F. R. Wagner, Yu. Grin, Int. J. Quantum Chem. 2006, 106, 1499.
72. M. Kohout, Program DGrid, Version 4.2, Dresden 2007.
73. R. Dennington II, T. Keith, J. Millam, K. Eppinnett, W. L. Hovell, R. Gilliland, GaussView, Version 3.09, Semichem Inc., Shawnee Mission KS, U.S.A., 2003.
74. N. E. Brese, M. O'Keeffe, Acta Crystallogr. 1991, B47, 192.
75. R. D. Shannon, Acta Crystallogr. 1976, A32, 751.
76. N. C. Norman, Chemistry of Arsenic, Antimony and Bismuth, 1st ed., Blackie Academic Professional, London, 1998.
77. a) E. Makovicky, W. G. Mumme, J. A. Watts, Can. Mineral. 1977, 15, 339;
78. b) W. G. Mumme, Neues Jahrb. Mineral. Monatsh. 1990, 193;
79. c) J.-H. Kim, D.-Y. Chung, D. Bilc, S. Loo, J. Short, S. D. Mahanti, T. Hogan, M. G. Kanatzidis, Chem. Mater. 2005, 17, 3606;
80. d) H. K. Herbert, W. G. Mumme, Neues Jahrb. Mineral. Monatsh. 1981, 69;
81. e) P. F. P. Poudeu, M. Ruck, Acta Crystallogr. 2005, C61, i41.
82. a) P. F. P. Poudeu, T. Söhnel, M. Ruck, Z. Anorg. Allg. Chem. 2004, 630, 1276;
83. b) M. Ruck, P. F. P. Poudeu, Z. Anorg. Allg. Chem. 2008, 634, 475;
84. c) M. Ruck, P. F. P. Poudeu, Z. Anorg. Allg. Chem. 2008, 634, 482.
85. H. Kalpen, W. Hönle, M. Somer, U. Schwarz, K. Peters, H. G. von Schnering, Z. Anorg. Allg. Chem. 1998, 624, 1137.