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Volumn 47, Issue 22, 2008, Pages 10211-10213

Chiral-layered metal phosphonate formed via spontaneous resolution showing dehydration-induced antiferromagnetic to ferromagnetic transformation

(4) Hou, Shou Zeng a Cao, Deng Ke a Li, Yi Zhi a Zheng, Li Min a

a NANJING UNIVERSITY (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 57149090286 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic801655a Document Type: Article

Times cited : (37)

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45
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- Crystals of dimensions 0.07 x 0.05 x 0.04 mm for 1 and 0.10 x 0.08 x 0.06 mm for 2 were selected for indexing and intensity data collection at room temperature on a Bruker SMART APEX CCD diffractometer equipped with graphite-monochromated Mo Kα (λ, 0.710 73 Å) radiation. Crystal data for 1: C7H11O4N 2PMn, monoclinic, space group P21, a, 5.0875(10) Å, b, 10.437(2) Å, c, 9.5129(19) Å, V, 505.09(17) Å3, Z, 2, Dc= 1.796 g cm-3, μ, 1.460 mm-1, F(000, 278. Unique reflections: 1731 Rint, 0.0357, Least-squares refinements were based on F2 and converged at R1, 0.0638 and wR2, 0.1266. Crystal data for 2: C7H11O4N 2PCd, orthorhombic, space group P212 121
- 2 and converged at R1 = 0.0278 and wR2 = 0.0745. CCDC 696826 and 696827 contain the supplementary crystallographic data for this paper.

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