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Volumn 47, Issue 13, 2008, Pages 5525-5527

Polymorphism in homochiral zinc phosphonates

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EID: 47949095076 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic800663t Document Type: Article

Times cited : (54)

References (26)

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22
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- Elem anal. Calcd, ) for C18H25ClN 2O6P2Zn2 (1, C, 36.42; H, 4.24; N, 4.72. Found: C, 36.33; H, 4.19; N, 4.62. IR (KBr, cm-1, 3429 (w, 3232 (w, 2981 (w, 1603 (w, 1456 (w, 1441 (w, 1272 (w, 1236 (m, 1199 (w, 1136 (s, 1095 (s, 1014 (s, 863 (w, 761 (m, 739 (w, 701 (m, 646 (w, 577 (m, 547 (w, 495 (w, Anal. Calcd for C18H 25ClN2O6P2Zn2 (2, C, 36.42; H, 4.24; N, 4.72. Found: C, 36.21; H, 4.33; N, 4.77. IR (KBr, cm -1, 3421 (w, 3231 (w, 2981 (w, 1602 (w, 1456 (w, 1441 (w, 1272 (w, 1236 (m, 1199 (w, 1136 (s, 1095 (s, 1004 (s, 862 (w, 761 (m, 739 (w, 701 (m, 636 (w, 577 (m, 547 (w, 495 (w, Anal. Calcd for C 18H25ClN2O6P2Zn 2 (3, C, 36.42; H, 4.24; N, 4.72. Found: C, 36.31; H, 4.30; N, 4.61. IR KBr, cm-1
- -1): 3440 (w), 3212 (w), 3031 (w), 2852 (w), 2394 (w), 1588 (w), 1454 (w), 1383 (w), 1275 (w), 1168 (m), 1133 (s), 1104 (s), 1079 (s), 1054 (s), 1007 (s), 815 (w), 763 (m), 740 (w), 701 (m), 633 (w), 613 (m), 572 (w).

23
- 47949085689
- Crystal data for 1: orthorhombic, P212 121, a, 8.979(1) Å, b, 10.000(1) Å c, 26.840(1) Å, V, 2410.1(3) Å3, Z, 4, ρcalcd, 1.636 g/cm3, μ, 2.270 mm-1, R1, 0.0367, wR2, 0.0524, GOF, 0.90. Crystal data for 2: orthorhombic, P212121, a, 8.9611(10) Å, b, 9.9772(12) Å, c, 26.791(3) Å, V, 2395.3(5) Å3, Z, 4, ρcalcd, 1.646 g/cm3, μ, 2.284 mm-1, R1, 0.0589, wR2, 0.1150, GOF, 1.02
- -1, R1 = 0.0589, wR2 = 0.1150, GOF = 1.02.

24
- 47949088374
- -1, R1 = 0.0623, wR2 = 0.1414, GOF = 1.09.
- -1, R1 = 0.0623, wR2 = 0.1414, GOF = 1.09.

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