Adducts of cyclodiphosph(V)azenes: Synthesis and structure

Zeitschrift fur Anorganische und Allgemeine Chemie

Volumn 634, Issue 8, 2008, Pages 1403-1408

  Hubrich, Christopher ^a   Michalik, Dirk ^a   Schulz, Axel ^a   Villinger, Alexander ^a  

^a UNIVERSITY OF ROSTOCK   (Germany)

Author keywords

Adduct compounds; Bonding; Crystal structures; Cyclodiphosphazenes

Indexed keywords

EID: 53849124335     PISSN: 00442313     EISSN: 15213749     Source Type: Journal    
DOI: 10.1002/zaac.200800106     Document Type: Article

References (34)

1. A. Baceiredo, G. Bertrand, J.-P. Majoral, G. Sicard, J. Jaud, J. Galy, J. Am. Chem. Soc. 1984, 106, 6088-6089.
2. See, for examples: a) R. H. Allcock, Chem. Rev. 1972, 72, 315;
3. b) M. Bermann, Top. Phosphorus Chem. 1972, 7, 311;
4. c) H. R. Allcock, Phosphorus-Nitrogen Compounds; Academic Press: New York, 1972;
5. d) A. W. Johnson, Ylides and Imines of Phosphorus; John Wiley & Sons: New York, 1993;
6. e) A. Steiner, S. Zacchini, P. I. Richards, Coord. Chem. Rev. 2002, 227, 193-216.
7. a) R. Wehmschulte, M. A. Khan, S. I. Hossain, Inorg. Chem. 2001, 40, 2756-2762;
8. b) J. Tirreé, D. Gudat, M. Nieger, E. Niecke, Angew. Chem. 2001 113, 3115-3117;
9. Angew. Chem. Int. Ed. 2001, 40, 3025-3028.
10. R. Ahlrichs, H. Schiffer, J. Am. Chem. Soc. 1985, 107, 6494-6498.
11. C. B. Fischer, S. Xu, H. Zipse, Chem. Eur. J. 2006, 12, 5779-5784.
12. C. P. Warrens, D. J. Woollins, Inorg. Synth. 1989, 25, 43-47.
13. a) G. M. Sheldrick, SHELXS-97: Program for the Solution of Crystal Structures, University of Göttingen, Germany 1997;
14. b) G. M. Sheldrick, SHELXL-97: Program for the Refinement of Crystal Structures, University of Göttingen, Germany 1997;
15. c) ABSPACK; Oxford Diffraction 2005;
16. d) G. M. Sheldrick, SADABS, Version 2. University of Göttingen, Germany 2004.
17. Compound 3 slowly decomposes at ambient temperatures and upon drying in vacuo. This is the reason why no accurate CHN data can be presented.
18. a) S. Herler, A. Villinger, J. Weigand, P. Mayer, A. Schulz, J. Schmedt auf der Günne, Angew. Chem. 2005, 117, 7968-7971;
19. Angew. Chem. Int. Ed. 2005, 44, 7790-7793;
20. b) P. Mayer, A. Schulz, A. Villinger, J. Organomet. Chem. 2007, 692, 2839-2842;
21. c) G. Fischer, S. Herler, P. Mayer, A. Schulz, A. Villinger, J. Weigand, Inorg. Chem. 2005, 44, 1740-1751;
22. d) P. Mayer, A. Schulz, A. Villinger, Chem. Commun. 2006, 1236-1238;
23. e) A. Schulz, A. Villinger, Angew. Chem. 2008, 120, 614-617;
24. Angew. Chem. Int. Ed. 2008, 47, 603-606.
25. a) N. Burford, T. S. Cameron, D. J. LeBlanc, P. Losier, S. Sereda, G. Wu, Organomet. 1997, 16, 4712-4717;
26. a) N. Burford, P. J. Ragogna, J. Chem. Soc., Dalton Trans. 2002, 4307-4315;
27. b) N. Burford, P. J. Ragogna, R. McDonald, M. J. Ferguson, J. Am. Chem. Soc. 2003, 125, 14404-14410;
28. N. Burford, D. E. Herbert, P. J. Ragogna, R. McDonald, M. J. Ferguson, J. Am. Chem. Soc. 2004, 126, 17067-17073.
29. K. Huynh, E. Rivard, A. J. Lough, I. Manners, Inorg. Chem. 2007, 46, 9979-9987.
30. a) Sum of covalent radii: r(P) = 1.1 and r(N) = 0.7; Holleman Wiberg, Lehrbuch der Anorganischen Chemie, 101. Aufl., Walter de Gruyter, 1995, Anhang V;
31. b) sum of covalent radii: r(Al) = 1.3 and r(N) = 0.7.
32. a) W. R. Nutt, J. S. Blanton, A. M. Boccanfusco, L. A. Silks III, A. R. Garber, J. D. Odom, Inorg. Chem. 1991, 30, 4136-4140;
33. b) H. Nöth, T. Seifert, Eur. J. Inorg. Chem. 2002, 602-612;
34. c) Ch. Hubrich, A. Schulz, A. Villinger, Z. Anorg. Allg. Chem. 2007, 633, 2362-2366.