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Macromolecules

Volumn 41, Issue 13, 2008, Pages 4856-4865

Effect of substrate geometry on polymer molecular weight and polydispersity during surface-initiated polymerization

(3) Gorman, Christopher B a Petrie, Randall J a,b Genzer, Jan a

a NORTH CAROLINA STATE UNIVERSITY (United States)

b BASF CORPORATION (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMI NUM OXIDE; AMERICAN CHEMICAL SOCIETY (ACS); CONFINEMENT EFFECTS; DIRECT ANALYSIS; HYDROGEN FLUORIDE (HF); INFRARED (IR); IONIZATION MASS SPECTROMETRY; MALDI-MS; MATRIX-ASSISTED LASER DESORPTION/IONIZATION (MALDI) MASS SPECTROMETRY; POLY(METHYL METHACRYLATE) (PMMA); POLYDISPERSE CHAINS; POLYMER CHAINS; POLYMER MOLECULAR WEIGHT; POLYMERIZATION CONDITIONS; SIGNAL TO NOISE RATIO (SNR); SUBSTRATE GEOMETRY; SURFACE INITIATED ATOM TRANSFER RADICAL POLYMERIZATION; SURFACE-INITIATED POLYMERIZATION (SIP); WEIGHT DISTRIBUTIONS;

ACRYLIC MONOMERS; ALUMINA; CHAINS; CHEMICAL REACTIONS; DESORPTION; ELECTRON BEAM LITHOGRAPHY; ESTERS; FREE RADICAL POLYMERIZATION; FREE RADICAL REACTIONS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROFLUORIC ACID; HYDROGEN; INFRARED SPECTROSCOPY; IONIZATION; LIGHT METALS; MASS SPECTROMETERS; MASS SPECTROMETRY; MATRIX ALGEBRA; MOLECULAR WEIGHT; MOLECULAR WEIGHT DISTRIBUTION; MONOMERS; NONMETALS; PHOTORESISTS; POLYACRYLATES; POLYMERIZATION; POLYMERS; POROUS SILICON; PULSED LASER DEPOSITION; SIGNAL TO NOISE RATIO; SILICON; SPECTROMETERS; SPECTROMETRY; SPECTROSCOPIC ANALYSIS; SPECTRUM ANALYSIS; SUBSTRATES;

ATOM TRANSFER RADICAL POLYMERIZATION;

EID: 47949109317 PISSN: 00249297 EISSN: None Source Type: Journal
DOI: 10.1021/ma8004857 Document Type: Article

Times cited : (95)

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- This approximate relation has been obtained by growing chains simultaneously in bulk and on the surface and determining M via size exclusion chromatography and h via ellipsometry. Although it has been found to be valid for a range of methacrylates and acrylates grown from BMPUS initiator layers deposited under identical conditions, this relationship should be considered as an estimate only because it assumes that chains grown under confinement possess the same rate of polymerization as those polymerized in solution. Nevertheless, this relationship provides a very reasonable estimate for the chain grafting density σ, σ ≈ 0.45 chains/nm2
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