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Inorganic Chemistry

Volumn 47, Issue 10, 2008, Pages 3937-3939

Heterobismetal complexes of [26]hexaphyrin(1.1.1.1.1.1)

(2) Mori, Shigeki a Osuka, Atsuhiro a

a KYOTO UNIVERSITY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 44349107106 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic8004147 Document Type: Article

Times cited : (50)

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- 3, Z = 4, R1 = 0.0670 [I > 2.0σ(I)], wR2 = 0.1682 (all data), GOF = 1.099 [I > 2.0σ(I)]. Only one of two structures is drawn in the figure, although both metal atoms are disordered.

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37
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- Although the mechanism of the high yield formation of 6 is not clear, the RhI salt is likely to act as a reductant to 2
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38
- 44349098968
- Crystallographic data of 5: C68H10N 6F30AuRh·2C2H3N, Mw, 1894.80, triclinic, P1 (No. 2, a, 15.110(4) Å, b, 15.121(5) Å, c, 15.498(5) Å, α, 88.653(13)°, β, 64.428(10)°, γ, 77.577(13)°, V, 3109.4(17) Å3, Dc, 2.024 g/cm3, Z, 2, R1, 0.0464 [I > 2.0σ(I, wR2, 0.1196 (all data, GOF, 1.045 [I > 2.0σI
- 3, Z = 2, R1 = 0.0464 [I > 2.0σ(I)] , wR2 = 0.1196 (all data), GOF = 1.045 [I > 2.0σ(I)].

39
- 44349119531
- Crystallographic data of 7: C76H18N 8F30AuRh·1.64C6H14·1. 86CHCl3, Mw, 2295.32, triclinic, P1 (No. 2, a, 17.223(4) Å, b, 17.784(7) Å, c, 18.132(6) Å, α, 105.845(13)°, β, 107.214(10)°, γ, 111.214(10)°, V, 4457(2) Å3, Dc, 1.724 g/cm3, Z, 2, R1, 0.0549 [I > 2.0σ(I, wR2, 0.1572 (all data, GOF, 1.063 [I > 2.0σI
- 3, Z = 2, R1 = 0.0549 [I > 2.0σ(I)], wR2 = 0.1572 (all data), GOF = 1.063 [I > 2.0σ(I)].

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