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The correlation length (ξ) has been calculated by fitting the peak with a Lorentzian distribution function and using the Scherrer equation as reported in ref 55: ξ = 0.89λ/(ω̄ COS θ), wherein λ is the wavelength of the X-rays, ω̄ is the full width at half maximum of the peak in radians, and θ is Bragg angle of the maximum of the peak.
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After shear alignment of the samples, all diffraction peaks split up in two opposing maxima that align in the same direction on the two-dimensional detector. See Supporting Information for details
-
After shear alignment of the samples, all diffraction peaks split up in two opposing maxima that align in the same direction on the two-dimensional detector. See Supporting Information for details.
-
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63
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41749123495
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The density of pure 1 was calculated at 100°C from the X-ray diffraction data. The value for PPI-dendr is the room temperature value reported by the supplier.
-
The density of pure 1 was calculated at 100°C from the X-ray diffraction data. The value for PPI-dendr is the room temperature value reported by the supplier.
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For example, the density of a 1:1 molar mixture of propionic acid (ρ = 0.993 g/mL) and ethanamine (ρ = 0.689 g/mL) is 1.018 g/mL at 27°C.
-
For example, the density of a 1:1 molar mixture of propionic acid (ρ = 0.993 g/mL) and ethanamine (ρ = 0.689 g/mL) is 1.018 g/mL at 27°C.
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