Ag, Ag2S, and Ag2Se nanocrystals: Synthesis, assembly, and construction of mesoporous structures

Journal of the American Chemical Society

Volumn 130, Issue 12, 2008, Pages 4016-4022

  Wang, Dingsheng ^a   Xie, Ting ^a   Peng, Qing ^a   Li, Yadong ^a  

^a TSINGHUA UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

MESOPOROUS MATERIALS; PYROLYSIS; SELF ASSEMBLY; SILVER COMPOUNDS; SYNTHESIS (CHEMICAL);

METAL-ORGANIC FRAMEWORKS (MOF); MOLECULAR BUILDING BLOCKS; MONODISPERSE NANOPARTICLES;

NANOCRYSTALS;

METAL; NANOCRYSTAL; NANOPARTICLE; OCTADECYLAMINE; ORGANIC COMPOUND; SELENIUM; SILVER; SILVER NITRATE; SULFUR;

ARTICLE; CHEMICAL COMPOSITION; DECOMPOSITION; DISPERSION; INDUSTRIAL PRODUCTION; POROSITY; SYNTHESIS;

EID: 41149117121     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja710004h     Document Type: Article

References (42)

1. Kresge, C. T.; Leonowicz, M. E.; Roth, W. J.; Vartuli, J. C.; Beck, J. S. Nature 1992, 359, 710.
2. Maschmeyer, T.; Rey, F.; Sankar, G.; Thomas, J. M. Nature 1995, 378, 159.
3. Tanev, P. T.; Pinnavaia, T. J. Science 1995, 267, 865.
4. Yang, P.; Deng, T.; Zhao, D.; Feng, P.; Pine, D.; Chmelka, B. F.; Whitesides, G. M.; Stucky, G. D. Science 1998, 282, 2244.
5. Kim, T. W.; Kleitz, F.; Paul, B.; Ryoo, R. J. Am. Chem. Soc. 2005, 127, 7601.
6. Hoffmann, F.; Cornelius, M.; Morell, J.; Fröba, M. Angew. Chem., Int. Ed. 2006, 45, 3216.
7. Lu, Y. F.; Fan, H. Y.; Stump, A.; Ward, T. L.; Rieker, T.; Brinker, C. J. Nature 1999, 398, 223.
8. Wan, Y.; Yang, H. F.; Zhao, D. Y. Acc. Chem. Res. 2006, 39, 423.
9. Tian, Z. R.; Tong, W.; Wang, J. Y.; Duan, N. G.; Krishnan, V. V.; Suib, S. L. Science 1997, 276, 926.
10. Yang, P. D.; Zhao, D. Y.; Margolese, D. I.; Chmelka, B. F.; Stucky, G. D. Nature 1998, 396, 152.
11. Jiao, F.; Jumas, J. C.; Womes, M.; Chadwick, A. V.; Harrison, A.; Bruce, P. G. J. Am. Chem. Soc. 2006, 128, 12905.
12. Lai, X. Y.; Li, X. T.; Geng, W. C.; Tu, J. C.; Li, J. X.; Qiu, S. L. Angew. Chem., Int. Ed. 2007, 46, 738.
13. Russell, V. A.; Evans, C. C.; Li, W. J.; Ward, M. D. Science 1997, 276, 575.
14. Li, H.; Eddaoudi, M.; O'Keeffe, M.; Yaghi, O. M. Nature 1999, 402, 276.
15. Eddaoudi, M.; Moler, D. B.; Li, H. L.; Chen, B. L.; Reineke, T. M.; O'Keeffe, M.; Yaghi, O. M. Acc. Chem. Res. 2001, 34, 319.
16. Eddaoudi, M.; Kim, J.; Rosi, N.; Vodak, D.; Wachter, J.; O'Keeffe, M.; Yaghi, O. M. Science 2002, 295, 469.
17. El-Kaderi, H. M.; Hunt, J. R.; Mendoza-Cortes, J. L.; Cote, A. P.; Taylor, R. E.; O'Keeffe, M.; Yaghi, O. M. Science 2007, 316, 268.
18. Braun, P. V.; Osenar, P.; Tohver, V.; Kennedy, S. B.; Stupp, S. I. J. Am. Chem. Soc. 1999, 121, 7320.
19. Shin, H. J.; Ryoo, R.; Liu, Z.; Terasaki, O. J. Am. Chem. Soc. 2001, 123, 1246.
20. Gao, F.; Lu, Q. Y.; Zhao, D. Y. Adv. Mater. 2003, 15, 739.
21. Mohanan, J. L.; Arachchige, I. U.; Brock, S. L. Science 2005, 307, 397.
22. Zhang, Y. X.; Zeng, H. C. J. Phys. Chem. C 2007, 111, 6970.
23. Klajn, R.; Bishop, K. J. M.; Fialkowski, M.; Paszewski, M.; Campbell, C. J.; Gray, T. P.; Grzybowski, B. A. Science 2007, 316, 261.
24. Xu, H.; Cui, L. L.; Tong, N. H.; Gu, H. C. J. Am. Chem. Soc. 2006, 128, 15582.
25. Sayle, D. C.; Mangili, B. C.; Klinowski, J.; Sayle, T. X. T. J. Am. Chem. Soc. 2006, 128, 15283.
26. Zhuang, J.; Wu, H.; Yang, Y.; Cao, Y. C. J. Am. Chem. Soc. 2007, 129, 14166.
27. Tao, A.; Sinsermsuksakul, P.; Yang, P. D. Angew. Chem., Int. Ed. 2006, 45, 4597.
28. Tao, A.; Sinsermsuksakul, P.; Yang, P. D. Nat. Nanotechnol. 2007, 2, 435.
29. Gao, F.; Lu, Q. Y.; Zhao, D. Y. Nano Lett. 2003, 3, 85.
30. Murray, C. B.; Norris, D. J.; Bawendi, M. G. J. Am. Chem. Soc. 1993, 115, 8706.
31. Peng, X. G.; Manna, L.; Yang, W. D.; Wickham, J.; Scher, E.; Kadavanich, A.; Alivisatos, A. P. Nature 2000, 404, 59.
32. Wang, X.; Zhuang, J.; Peng, Q.; Li, Y. D. Nature 2005, 437, 121.
33. Habas, S. E.; Lee, H.; Radmilovic, V.; Somorjal, G. A.; Yang, P. D. Nat. Mater. 2007, 6, 692.
34. Yin, Y. D.; Li, Z. Y.; Zhong, Z. Y.; Gates, B.; Xia, Y. N.; Venkateswaran, S. J. Mater. Chem. 2002, 12, 522.
35. Lin, X. Z.; Teng, X.; Yang, H. Langmuir 2003, 19, 10081.
36. Hambrock, J.; Becker, R.; Birkner, A.; Weib, J.; Fischer, R. A. Chem. Commun. 2002, 68.
37. Son, S. U.; Park, I. K.; Park, J.; Hyeon, T. Chem. Commun. 2004, 778.
38. See Supporting Information.
39. 2Se: Wiegers, University Bloemsingel 10, Groningen, The Netherlands, Private Communication, 1972. The quality of the XRD pattern of Ag nanocrystals is influenced by peak broadening. However, the XRD pattern of calcined Ag spheres (see Supporting Information) can help us to further identify Ag crystal structure.
40. 2Se nanoparticles are monocrystals.
41. Bai, F.; Wang, D. S.; Huo, Z. Y.; Chen, W.; Liu, L. P.; Liang, X.; Chen, C.; Wang, X.; Peng, Q.; Li, Y. D. Angew. Chem., Int. Ed. 2007, 46, 6650.
42. 2S nanoparticles can also assemble into superlattices with a diameter of 200 nm.