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note
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38: C, 13.75%; H, 3.23%; N, 6.41%. Found: C, 13.71%; H, 3.05%; N, 6.38%. IR: 3326 (w), 3180 (m), 1662 (m), 1624 (s), 1543 (m), 1477 (s), 1382 (m), 1328 (m), 1246 (m), 1170 (m), 995 (m), 891 (s), 796 (w), 767 (m), 620 (m).
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47
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35348820935
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note
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2 by full-matrix least-squares using the SHELXTL-97 program package. All non-hydrogen atoms were refined anisotropically. The organic hydrogen atoms were generated geometrically and hydrogen atoms of water molecules were located in a difference map and refined with the distance restraint O-H = 0.85(1) Å.
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