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Chemistry Letters

Volumn 36, Issue 3, 2007, Pages 356-357

Inorganic-organic hybrid with 3D supramolecular channel assembled through C-H⋯O interactions based on the decavanadate

(5) Li, Taohai a,b Lü, Jian a,b Gao, Shuiying a Li, Feng a,b Cao, Rong a

a FUJIAN INSTITUTE OF RESEARCH ON THE STRUCTURE OF MATTER (China)

b UNIVERSITY OF CHINESE ACADEMY OF SCIENCES (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 34047266207 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2007.356 Document Type: Article

Times cited : (18)

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- Preparation of 1: The starting materials K2[H 4V10O28]·7H2O (0.5 mmol, Cu(NO3)3·6H2O (0.5 mmol, 2,2′-bipy (1 mmol, and H2O (9.0 mL) in a molar ration 1:1:2:1000 were mixed. The resulting suspension was stirred for 1 h, with sufficient HNO3 to adjust the pH to 4.5, sealed in a 20 mL Teflon-lined reactor and heated at 160°C for four days. Then, the autoclave was cooled at 6°C/h to room temperature. Blue block crystals of compound 1 were filtered, washed with water, and dried at ambient temperature (yield 51, based on vanadium, Anal. Calcd for C50H44N 10O29V10Cu2 (1885.44, C, 31.85; H, 2.35; N, 7.43; Cu, 6.74; V, 27.02, Found: C, 31.75; H, 2.20, N, 7.63; V, 27.23; Cu, 6.58, IR (KBr pellets, v/cm-1, 1613(s, 1470(m, 1442(m, 1394(w, 1017(m, 962(s, 883(vs, 840s, 7
- -1): 1613(s), 1470(m), 1442(m), 1394(w), 1017(m), 962(s), 883(vs), 840(s), 719(m), and 664(w).

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- Crystal data for 1: C50H44N10O 29V10Cu2, Mr, 1885.44, Triclinic, a, 10.006(5, b, 13.046(6, c, 13.085(6) Å, V, 1545.72(12) Å3, T, 293(2) K, space group P1̄, Z, 2, μ, 1.320 mm-1, 5394 reflections measured, 455 independent (Rint, 0.0286, R1, 0.0766(I > 2σ(I, WR2, 0.1452 all data, CCDC: 619516
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