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-1): 3410(s), 3021(w), 2850(w), 2489(w), 1628(s), 1573(m), 1519(w), 1473(s), 1384(m), 1355(w), 1306(m), 1271(m) 1185(w), 1148(w), 1102(w), 1036(w), 946(m), 900(w), 834(w), 812(m), 784(m), 754(m), 670(w), 629(w), 581(w), 543(w), 512(w), 490(w).
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2 = 0.2387. The refinements revealed the twofold disordered aqua oxygen atoms (O19, O21) in the structure. The disordered guest aqua molecules were refined in two orientations (O19, O19′; O21, O21′), located from the difference Fourier map at the final states of refinements.
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