Synthesis and characterization of a polyoxovanadate cluster representing a new topology

Chemical Communications

Volumn , Issue 37, 2005, Pages 4658-4660

  Khan, M Ishaque ^a   Ayesh, Samar ^a   Doedens, Robert J ^b   Yu, Minghui ^c   O'Connor, Charles J ^c  

^a Illinois Institute of Technology   (United States)

^b UNIVERSITY OF CALIFORNIA   (United States)

^c UNIVERSITY OF NEW ORLEANS   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CHLORIDE ION; POLYOXOVANADATE; UNCLASSIFIED DRUG; VANADIUM DERIVATIVE;

ARTICLE; CHEMICAL ANALYSIS; CRYSTAL STRUCTURE; CRYSTALLIZATION; MAGNETISM; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 26944455534     PISSN: 13597345     EISSN: None     Source Type: Journal    
DOI: 10.1039/b507531a     Document Type: Article

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25. The magnetic data were recorded on a 39.2 mg polycrystalline sample of 1 in the 2-300 K temperature range using a Quantum Design MPMS-5S SQUID spectrometer. Calibrating and operating procedures have been reported elsewhere [C. J. O'Connor, Prog. Inorg. Chem., 1979, 29, 203]. The temperature dependent magnetic data were obtained at a magnetic field of H = 1000 Oe, and the diamagnetic background from the sample holder was corrected.
26. -1.