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Volumn 9, Issue 18, 2007, Pages 3495-3498

The first N-heterocyclic carbene-based nickel catalyst for C-S coupling

Author keywords

[No Author keywords available]

Indexed keywords

CARBENE; CARBON; DRUG DERIVATIVE; HETEROCYCLIC COMPOUND; HYDROCARBON; METHANE; NICKEL; NITROGEN; SULFUR; TRANSITION ELEMENT;

EID: 34548527662     PISSN: 15237060     EISSN: None     Source Type: Journal    
DOI: 10.1021/ol071248x     Document Type: Article
Times cited : (346)

References (63)
  • 28
    • 0003491250 scopus 로고
    • For general reviews on sulfides, see:, Jones, D. N, Ed, Pergamon Press: Oxford
    • For general reviews on sulfides, see: Comprehensive Organic Chemistry; Jones, D. N., Ed.; Pergamon Press: Oxford, 1979; Vol. 3.
    • (1979) Comprehensive Organic Chemistry , vol.3
  • 43
    • 33745685986 scopus 로고    scopus 로고
    • For Cu catalysts: (a) Kumar, S.; Engman, L. J. Org. Chem. 2006, 71, 5400.
    • For Cu catalysts: (a) Kumar, S.; Engman, L. J. Org. Chem. 2006, 71, 5400.
  • 49
    • 34548526504 scopus 로고    scopus 로고
    • For Ni catalysts: (a) Cristau, H. J.; Chabaud, B.; Chene, A.; Christol, H. Synthesis 1981, 1892.
    • For Ni catalysts: (a) Cristau, H. J.; Chabaud, B.; Chene, A.; Christol, H. Synthesis 1981, 1892.
  • 53
    • 33846010734 scopus 로고    scopus 로고
    • For Co catalysts: Wong, Y.-C.; Jayanth, T. T.; Cheng, C.-H. Org. Lett. 2006, 8, 5613.
    • For Co catalysts: Wong, Y.-C.; Jayanth, T. T.; Cheng, C.-H. Org. Lett. 2006, 8, 5613.
  • 60
    • 34548526030 scopus 로고    scopus 로고
    • t3u (0.6 mmol) in 10 mL of DMF. The mixture was stirred for 1 h at room temperature, and used as the catalyst stock solution for catalytic reactions.
    • t3u (0.6 mmol) in 10 mL of DMF. The mixture was stirred for 1 h at room temperature, and used as the catalyst stock solution for catalytic reactions.
  • 61
    • 34548525652 scopus 로고    scopus 로고
    • tBu (125 mg, 1.1 mmol), thiophenol (1.05 mmol), and 4-bromotoluene (1 mmol) were mixed with 3 mL of DMF in a reaction vial. The vial was capped, and the reaction mixture was stirred at 110°C for 16 h. Yields were measured by gas liquid chromatography (GLC) and isolation of pure product. Products were confirmed by gas chromatography-mass spectrometry (GC-MS) and nuclear magnetic resonance (NMR).
    • tBu (125 mg, 1.1 mmol), thiophenol (1.05 mmol), and 4-bromotoluene (1 mmol) were mixed with 3 mL of DMF in a reaction vial. The vial was capped, and the reaction mixture was stirred at 110°C for 16 h. Yields were measured by gas liquid chromatography (GLC) and isolation of pure product. Products were confirmed by gas chromatography-mass spectrometry (GC-MS) and nuclear magnetic resonance (NMR).
  • 62
    • 0346387650 scopus 로고    scopus 로고
    • Kurosawa, H, Yamamoto, A, Eds, Elsevier: Amsterdam, The Netherlands
    • (a) Komiya, S.; Hirano, M. In Fundamentals of Molecular Catalysis; Kurosawa, H., Yamamoto, A., Eds.; Elsevier: Amsterdam, The Netherlands, 2003.
    • (2003) Fundamentals of Molecular Catalysis
    • Komiya, S.1    Hirano, M.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.