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For the latest works see: a, Davidson, M. G, Hughes, A. K, Marder, T. B, Wade K, Eds, Royal Society of Chemistry: Cambridge, U.K
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23
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34547508678
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In order to determine what is the fate of the bridging endo hydrogen atom of salts 1 during their transformations to complexes 5 and 6, we have synthesized a sample of [Cs][10-endo-D-7,8-(4′-MeC6H 4)2-7,8-nido-C2B9H9, 9) with a high degree of monodeuteration (ca 83, by the method of Hawthorne et al.7 and studied the metalation reaction of 9 with 3 under the experimental conditions described for the non-deuterated analogue. An examination of the deuterated pseudocloso complex thus obtained by the comparison of its 2H NMR spectrum with the 1{11B} NMR spectrum of 5 (see the Supporting Information) provided evidence for the presence of the endo deuterium atom in this species mostly on C(4)-C(8) carbon atoms of the carbocyclic C8 ring
-
8 ring.
-
-
-
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24
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33947292130
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Howe, D. E.; Jones, C. J.; Wiersema, R. J.; Hawthorne, M. F. Inorg. Chem. 1971, 10, 2516.
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0001101373
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26
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0001700409
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(b) Behnken, P. E.; Marder, T. B.; Baker, R. T.; Knobler, C. B.; Thompson, M. R.; Hawthorne, M. F. J.Am. Chem. Soc. 1985, 107, 932.
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27
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0007174864
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(c) Chizhevsky, I. T.; Zinevich, T. V.; Petrovskii, P. V.; Antonovich, V. A.; Zakharkin, L. I. Metalloorg. Khim. 1991, 4, 1411;
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28
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34547500876
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Organomet. Chem. USSR (Engl. Transl.) 1991, 4, 703.
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Organomet. Chem. USSR (Engl. Transl.) 1991, 4, 703.
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31
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0042863044
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Chizhevsky, I.T.6
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32
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6344257044
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(g) Safronov, A. V.; Zinevich, T. V.; Dolgushin, F. M.; Tok, O. L.; Vorontsov, E. V.; Chizhevsky, I. T. Organometallics 2004, 23, 4970.
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33
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Hodson, B. E.; McGrath, T. D.; Stone, F. G. A. Organometallics 2005, 24, 1638.
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Teixidor, F.; Flores, M. A.; Viñas, C; Sillanpää, R.; Kivekäs, R. J.Am. Chem. Soc 2000, 122, 1963.
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Teixidor, F.1
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35
-
-
34547543738
-
-
3g no further details, as far as we are aware, have been reported.
-
3g no further details, as far as we are aware, have been reported.
-
-
-
-
36
-
-
0007882582
-
-
See for example: a
-
See for example: (a) Esteruelas, M. A.; Olivan, M.; Oro, L. A.; Schutz, M.; Sola, E.; Werner, H. Organometallics 1992, 11, 3659.
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Esteruelas, M.A.1
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Sola, E.5
Werner, H.6
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37
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27644494626
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(b) Kaduk, J. A.; Poulos, A. T.; Ibers, J. A. J.Organomet. Chem. 1977, 127, 245.
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Kaduk, J.A.1
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38
-
-
34547513378
-
-
11B chemical shifts reported in the text of ref 5e for the compound 2 is in error and should be read as +6.15 ppm.
-
11B chemical shifts reported in the text of ref 5e for the compound 2 is in error and should be read as +6.15 ppm.
-
-
-
-
39
-
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19544380072
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McIntosh, R.; Ellis, D.; Gil-Lostes, J.; Dalby, K. J.; Rosair, G. M.; Welch A. J.Dalton Trans. 2005, 1842.
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1131. For the latest reviews see
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(h) Boyd, A. S. F.; Burke, A.; Ellis, D.; Ferrer, D.; Giles, B. T.; Laguna, M. A.; McIntosh, R.; Macgregor, S. A.; Ormsby, D. L.; Rosair, G. M.; Schmidt, F.; Wilson, N. M. M.; Welch, A. J.Pure Appl. Chem. 2003, 75, 1325.
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49
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34547553287
-
-
Further experiments to attempt to find more powerful methods for the preparation of 7 and/or its derivatives and studies designed to establish the mechanism of formation of 7 are currently underway in our laboratory
-
Further experiments to attempt to find more powerful methods for the preparation of 7 and/or its derivatives and studies designed to establish the mechanism of formation of 7 are currently underway in our laboratory.
-
-
-
-
50
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34547546499
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(a) Kim, J.-H.; Lambrani, M.; Hwang, J.-W.; Do, Y. J.Chem. Soc., Chem. Commun. 1997, 1761.
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34547535179
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Sheldrick, G. M. SHELXTL-97, Version 5.10; Bruker AXS Inc, Madison, WI, 1997
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Sheldrick, G. M. SHELXTL-97, Version 5.10; Bruker AXS Inc., Madison, WI, 1997.
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