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Volumn 349, Issue 7, 2007, Pages 1256-1264

A microwave-enhanced, lewis acid-catalyzed synthesis of 1,3-dioxolanes and oxazolines from epoxides

Author keywords

Dioxolanes; Epoxides; Lactams; Lewis acids; Microwave heating

Indexed keywords


EID: 34547147015     PISSN: 16154150     EISSN: 15213897     Source Type: Journal    
DOI: 10.1002/adsc.200600516     Document Type: Article
Times cited : (13)

References (48)
  • 8
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    • For a review see
    • For a review see: F. A. J. Meskens, Synthesis 1981, 7, 501-522.
    • (1981) Synthesis , vol.7 , pp. 501-522
    • Meskens, F.A.J.1
  • 19
    • 12344294418 scopus 로고    scopus 로고
    • c) J. W. Clader, Science 2004, 303, 1201-1204;
    • (2004) Science , vol.303 , pp. 1201-1204
    • Clader, J.W.1
  • 25
    • 33846014265 scopus 로고    scopus 로고
    • Microwave Synthesis: Chemistry at the Speed of Light
    • 1st edn, NC
    • d) B. L. Hayes, Microwave Synthesis: Chemistry at the Speed of Light, 1st edn., CEM Publishing, Matthews, NC, 2002.
    • (2002) CEM Publishing, Matthews
    • Hayes, B.L.1
  • 27
    • 34547210948 scopus 로고    scopus 로고
    • Crystal data for 2a have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no
    • Crystal data for 2a have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 286004.
    • , vol.CCDC 286004
  • 28
    • 34547230897 scopus 로고    scopus 로고
    • Boiling point 130-131°C.
    • Boiling point 130-131°C.
  • 29
    • 34547174456 scopus 로고    scopus 로고
    • In some cases, a small amount of diol could be isolated from flash chromatography
    • In some cases, a small amount of diol could be isolated from flash chromatography.
  • 30
    • 34547177003 scopus 로고    scopus 로고
    • Crystal data for 5a have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no
    • Crystal data for 5a have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC 621038.
    • , vol.CCDC 621038
  • 38
    • 34547228942 scopus 로고    scopus 로고
    • The presence of the diol is due to the hydrolysis of the corresponding cyclic acetal, since treatment of cyclohexene oxide with the catalyst in the presence of water did not afford direct transformation of epoxide to diol
    • The presence of the diol is due to the hydrolysis of the corresponding cyclic acetal, since treatment of cyclohexene oxide with the catalyst in the presence of water did not afford direct transformation of epoxide to diol.
  • 42
    • 27744548947 scopus 로고    scopus 로고
    • for compound 10 see: YS. Trudeau, J. B. Morgan, M. Shrestha, J. P. Morken, J. Org. Chem. 2005, 70, 9538-9544.
    • c) for compound 10 see: YS. Trudeau, J. B. Morgan, M. Shrestha, J. P. Morken, J. Org. Chem. 2005, 70, 9538-9544.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.