Analysis of polycyclic aromatic hydrocarbons in vegetable oils combining gel permeation chromatography with solid-phase extraction clean-up

Food Additives and Contaminants

Volumn 24, Issue 7, 2007, Pages 758-767

  Fromberg, A ^a   Hojgard A ^b   Duedahl Olesen, L ^a  

^a TECHNICAL UNIVERSITY OF DENMARK   (Denmark)

^b Regional Veterinary and Food Administration Centre   (Denmark)

Author keywords

Analysis; Benzo a pyrene; Gel permeation chromatography; Grape seed oil; Method validation; Polycyclic aromatic hydrocarbons (PAHs); Rapeseed oil; Sesame oil; Solid phase extraction; Sunflower oil; Vegetable oil

Indexed keywords

BENZO[A]PYRENE; EDIBLE OIL; OLIVE OIL; POLYCYCLIC AROMATIC HYDROCARBON; RAPESEED OIL; SESAME SEED OIL; SILICON DIOXIDE; SUNFLOWER OIL; VEGETABLE OIL;

ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; EUROPE; FOOD CONTAMINATION; GAS CHROMATOGRAPHY; GEL PERMEATION CHROMATOGRAPHY; MARKET; MASS SPECTROMETRY; MATERIALS HANDLING; PRIORITY JOURNAL; SOLID PHASE EXTRACTION; TOXIN ANALYSIS;

CHROMATOGRAPHY, GEL; DIETARY FATS, UNSATURATED; FOOD ANALYSIS; FOOD CONTAMINATION; POLYCYCLIC HYDROCARBONS, AROMATIC;

BRASSICA NAPUS; HELIANTHUS; SESAMUM INDICUM; VITACEAE;

EID: 34447302544     PISSN: 0265203X     EISSN: 14645122     Source Type: Journal    
DOI: 10.1080/02652030601150505     Document Type: Article

References (25)

1. Bolt, DB, Bradley, JC and Re, MA (1997) The preparation of 13C-labeled standards of polycyclic aromatic hydrocarbons and other micropollutants: Synthetic and QA/QC considerations. Chemosphere, 34, pp. 905-913.
2. Danak (2003)
3. Dennis, MJ, Massey, RC, Cripps, G., Venn, I., Howarth, N. and Lee, G. (1991) Factors affecting the polycyclic aromatic hydrocarbon content of cereals, fats and other food products. Food Additives and Contaminants, 8, pp. 517-530.
4. European Commission (2002) Opinion of the Scientific Committee on Food on the risks to human health of polycyclic aromatic hydrocarbons in food
5. European Commission (2004) Report on experts participating in Task 3.2.12. Collection of occurrence data on polycyclic aromatic hydrocarbons in food
6. European Commission (2005) Commission Directive 2005/10/EC of 4 February 2005 laying down sampling methods and the methods of analysis for the official control of the levels of benzo. [a] pyrene in foodstuffs. Official Journal of the European Union, 34:15
7. European Commission (2005) Commission recommendation of 4 February 2005 on further investigation into the levels of polycyclic aromatic hydrocarbons in certain foods. Official Journal of the European Union, 34:43
8. European Commission (2005) Commission Regulation (EC) No. 208/2005 of 4 February 2005 amending Regulation (EC) No 466/2001 as regards polycyclic aromatic hydrocarbons. Official Journal of the European Union, 34:3
9. FAPAS (2004) Environmental contaminants FAPAS® Series 6 Round 18, UK
10. Hopia, A., Pyysalo, H. and Wickström, K. (1986) Margarines, butter and vegetable oils as sources of polycyclic aromatic hydrocarbons. Journal of the American Oil Chemists' Society, 63, pp. 889-893.
11. Horwitz, W. (1982) Evaluation of analytical methods used for regulation of foods and drugs. Analytical Chemistry, 54, pp. 67A-76A.
12. International Programme on Chemical Safety (IPCS) (1998) Selected non-heterocyclic polycyclic aromatic hydrocarbons. Environmental Health Criteria No. 202, World Health Organisation, Geneva
13. (1993) BIPM, IEC, IFCC, ISO, IUPAC, IUPAP, OIML guide to the expression of uncertainty in measurement, ISO, Geneva
14. (2005) General requirements for the competence of testing and calibration laboratories, ISO, Geneva
15. Larsson, BK, Eriksson, AT and Cervenka, M. (1987) Polycyclic aromatic hydrocarbons in crude and deodorized vegetable oils. Journal of American Oil Chemist's Society, 64, pp. 365-370.
16. Lodovici, M., Dolara, P., Casalini, C., Ciappellano, S. and Testolin, G. (1995) Polycyclic aromatic hydrocarbon contamination in the Italian diet. Food Additives and Contaminants, 12, pp. 703-713.
17. McClure, FD and Lee, JK (2003) Computation of HORRAT values. Journal of AOAC International, 86, pp. 1056-1058.
18. Menichini, E., Bocca, A., Merli, F., Ianni, D. and Monfredini, F. (1991) Polycyclic aromatic hydrocarbons in olive oils on the Italian market. Food Additives and Contaminants, 8, pp. 363-369.
19. Moret, S. and Conte, LS (2000) Polycyclic aromatic hydrocarbons in edible fats and oils: Occurrence and analytical methods. Review. Journal of Chromatography, 882, pp. 245-253.
20. Moret, S., Dudine, A. and Conte, LS (2000) Processing effects on the polyaromatic hydrocarbon content of grapeseed oil. Journal of the American Oil Chemists' Society, 77, pp. 1289-1292.
21. Moret, S., Piani, B., Bortolomeazzi, R. and Conte, LS (1997) HPLC determination of polycyclic aromatic hydrocarbons in olive oils. Zeitschrift für Lebensmittel Untersuchung und -Forschung A, 205, pp. 116-120.
22. Pupin, AM and Toledo, MCF (1996) Benzo[a]pyrene in olive oils on the Brazilian market. Food Chemistry, 55, pp. 185-188.
23. Speer, K., Steeg, E., Horstmann, P., Kühn, Th and Montag, A. (1990) Determination and distribution of polycyclic aromatic hydrocarbons in native vegetable oils, smoked fish products, mussels and oysters, and bream from the river Elbe. Journal of High Resolution Chromatography, 13, pp. 104-111.
24. Swetman, T., Head, S. and Evans, D. (1999) Contamination of coconut oil by PAH. Inform-International News on Fats Oils and Related Materials, 10, pp. 706-712.
25. Van der Wielen, JCA, Jansen, JTA, Martena, MJ, De Groot, HN and Veld, PH In't (2006) Determination of the level of benzo[a]pyrene in fatty foods and food supplements. Food Additives and Contaminants, 23, pp. 709-714.